A simplified scheme, combining aspects of the classical fire-assay with an atomic-absorption finish, is presented for the determination of gold and silver in ores and concentrates. The lead assay button is scorified to approximately 2 g and then parted in nitric acid. The filtrate is analysed by AAS for silver; the residue is dissolved in aqua regia and subsequently analysed for gold by AAS. Th...

Spark source mass spectrometry (SSMS) and atomic absorption spectrometry (AAS) have played important roles as powerful analytical tools. Both these techniques have undergone significant improvements since the late fifties in instrumentation and methodology leading to their application in various branches of science and te chnology. These techniques can be regarded as complementary techniques in...

We realize a continuous, intense, cold molecular and atomic beam source based on buffer-gas cooling. Hot vapor (up to 600K) from an oven is mixed with cold (15K) neon buffer gas, and then emitted into a high-flux beam. The novel use of cold neon as a buffer gas produces a forward velocity distribution and low-energy tail that is comparable to much colder helium-based sources. We expect this sou...

The use of clay materials for the production of emulsion paints was investigated. Two types of clay: White tinged with Purple and Smooth clay (WSP) and Grey Brown and Coarse clay (GBC), were used for the production of Emulsion Clay Paints (ECP). Conventional Chemical pigmented Paint (CP) was also produced as a control. Atomic Absorption Spectroscopy, (AAS) was used to determine the chemical com...

A novel lignosilicate (LS) composite was synthesized from pre-extracted (hot water, 80% ethanol, 0.3 N NaOH) lignin of rice husk (RH) using TEOS as matrix. The extracted lignins were subjected to surface modification by acetylation followed by in situ synthesis of lignosilicate (LS) composites by sol-gel method for application in nickel removal. LS were characterized by FT-IR, scanning electron...

Extracellular Polysaccharides (EPS) from both prokaryotes and eukaryotes have a great deal of research interest as they protect the producer from different stresses including antibiotics, ionic stress, desiccation and assist in bio-film formation, pathogenesis, adhesion, etc. In this study haloalkaliphilic Bacillus sp., known to cope with osmophilic stress, was selected and screened for EPS pro...

So far, no research has been focused on the determination of organomercuries in sewage sludge. Here, an ultrasonic extraction method for the rapid determination of methylmercury (MeHg) and ethylmercury (EtHg) in sewage sludge after ultrasound-assisted extraction is proposed. Using TMA (tetramethylammonium hydroxide) as the extractant with 3.0 g copper powder, ultrasonic extraction for 30 min at...