A novel method of preparing thermally stable zirconia-based mesoporous materials was developed. The zirconia-based mesoporous materials of 2D-hexagonal structure were prepared using zirconium sulfate as the zirconium precursor and cetyltrimethylammonium (CTMA) as the pore-directing agent with the aid of salt in the synthesis solution to reduce the sulfate content in the final product and signif...

Co-precipitated Cu-MgO catalysts were prepared and evaluated for the gas-phase hydrogenation of furfural. The effect of heating rate at the calcination step was studied by comparing the performance of three catalysts prepared via the same procedure but calcined at different heating rates. The results established that altering the heating rate could influence the structural properties of the cat...

Cobalt Oxide/ Zinc Oxide nanocomposite was synthesized by dropwise addition ofCo(NO)3.6H2O and Zn(NO3)2.4H2O solutions to KOH solution at different temperatures followed bycalcination at 300ºC for 4 h. The morphology and structure of nanoparticles and the influence oftemperature on particle size were studied using scanning electron microscopy (SEM) and X-RayDiffraction (XRD). Minimum particle s...

The nano-crystalline nickel-zinc ferrite was prepared via chemical synthesis. Zinc nitrate, nickel nitrate, iron nitrate hydrate, citric acid and ethylene glycol were used as precursor materials. Crystallization behavior of the precursor was studied by X-ray diffraction (XRD). Nanoparticle phases can change amorphous to spinel ferrite depending on the calcination temperature and crystallite siz...

Rapid thermal treatments potentially allow for a significant reduction in production time of ceramic multilayered membranes, in turn aiding increased industrial application of these membranes and accelerating research on their development. Two methods are proposed for the rapid thermal treatment of thin supported inorganic membrane films. Both methods involve an instant increment in temperature...

Quantitative determination of Br?nsted acid sites in acidic mordenite samples with varying proton concentrations has been studied using aqueous conductometric titration method. Conductometric titration of the ammonium form of mordenite with sodium hydroxide is feasible and the results indicate potential number of Br?nsted acid sites. However, Br?nsted acid sites concentration in acidic mordenit...

in this study the characteristics of two different kinds of la0.6sr0.4co0.2fe0.8o3 (lscf) powders, one in-house synthesized powder by a co-precipitation method and another one purchased from fuel cell materials co. (fcm co., usa), were compared. the co-precipitated powder was prepared by using ammonium carbonate as precipitant with a nh4+/no3- molar ratio of 2 and calcination at 1000c for 1 h....