1. Serum bile acids in seven patients with adult type myotonic dystrophy and 22 normal persons were quantitatively analysed by gas-liquid chromatography and gas chromatography-mass spectrometry for cholesterol, gamma-glutamyltransferase and bilirubin. There was no bile obstruction in any patient. 2. Dexoycholic acid values in all mothers of patients with congenital type myotonic dystrophy were ...

194 CLINICAL CHEMISTRY, Vol. 25, No. 1, 1979 gas chromatography before and after acid (6 mol/L HC1) and alkaline (NaOH) hydrolysis. We frequently observe a peak in the lactic acid position after alkaline hydrolysis. After acid hydrolysis of the same urine no lactate isobserved, but a peak appears in the position of levulinic acid. The mass spectra of these two peaks were identical with those of...

The Phlomis bracteosa oil constituents of methyl ester derivatives of fatty acids were analyzed using Gas Chromatography coupled to mass spectrometer. The results obtained containing the saturated as well as unsaturated fatty acids of P. bracteosa oils. A total of 18 different components were identified and quantified. Methyl ester of octadecadienoic acid was found in high concentration 6.88 %,...

A gas-liquid chromatographic procedure has been developed to quantitate dipicolinic acid in bacterial spores. The culture, washed from a plate, was hydrolyzed with acid containing the internal standard, pyridine-2,4-dicarboxylate, and then extracted into methyl isobutyl ketone. The internal standard and dipicolinic acid were then extracted into a small volume of trimethylphenylammonium hydroxid...

In this study, we examined the disposition, metabolism, and excretion of a novel cardioprotective agent, 3-(2,2, 2-trimethylhydrazinium)propionate dihydrate (MET-88), in rats. The disposition of MET-88 after oral and i.v. administration of 2, 20, and 60 mg/kg indicated that the pharmacokinetics of MET-88 were nonlinear. The profiles of radioactive MET-88 and total radioactivity in plasma were c...

An annular denuder system, which consisted of a cyclone separator; two diffusion denuders coated with sodium carbonate and citric acid, respectively; and a filter pack consisting of Teflon and nylon filters in series, was used to measure acid gases, ammonia (NH3), and fine particles in the atmosphere from April 1998 to March 1999 in eastern North Carolina (i.e., an NH3-rich environment). The so...

the pomegranate seeds of four iranian commercial varieties  (abanmahi (ab), malas (ms), pust sefid (ps) and shahvar (sh)) were evaluated in terms of some quality properties including protein, oil, dietary fiber, mineral contents and fatty acid composition. physicochemical properties and antioxidant activity of pomegranate seed oils (psos) were also determined. the oil antioxidant activity was m...