نتایج جستجو برای: 34dihydropyrimidin 21h thiones
تعداد نتایج: 751 فیلتر نتایج به سال:
In this work, it was of interest to synthesize new series of some 2-[(E)-2-furan-2-yl-vinyl]-quinazolin-4(3H)-ones incorporated into pyrazoline, isoxazoline, pyrimidine or pyrimidine-thione ring systems at position-3 of the quinazoline ring. The antimicrobial activity and antiinflammatory effect of some of these compounds were studied.
In the title compound, C19H16N4S, the pyrazolo-[3,4-d]pyrimidine ring is close to being planar, with the greatest deviation from the mean plane being 0.023 (2) Å for the C atom bearing the thione S atom. The two phenyl rings are nearly perpendicular to the fused ring system [dihedral angles = 71.4 (2) and 78.1 (2)°], but are oriented in opposite directions; the dihedral angle between the phenyl...
In the title compound, C(14)H(14)N(2)OS(2), the furan ring exhibits rotational disorder over two orientations, with an occupancy ratio of 0.508 (7):0.492 (7). The furan and phenyl rings form dihedral angles of 8.2 (6) (major occupancy component), 14.8 (6) (minor occupancy component) and 73.65 (9)°, respectively, with the central residue (C(4)N(2)S(2)), indicating a twisted conformation for the ...
In the last few years we demonstrated the utility of the phthalimidesulfenyl chloride (PhthNSCl, Phth = Phthaloyl) mediated generation of α,α’-dioxothiones and several related thiocarbonyl species. These reactive thione derivatives can be used as efficient electron-poor dienes in inverse electron demand Diels-Alder reactions with a plethora of electron rich alkenes, giving rise to interesting s...
Pyridinethiones are important ligand precursors of coordination complexes of therapeutic value. In aqueous solution, pyridinethiones can dimerize and tautomerize to the corresponding thiols. However, the tautomerism of pyridinethiones, which can impact on therapeutic performance, is yet not fully understood. To resolve this important issue, we have carried out ab initio and DFT calculations to ...
We report here an efficient and green method for Biginelli condensation reaction of aldehydes, β-ketoesters and urea or thiourea catalyzed by Brønsted acidic ionic liquid [Btto][p-TSA] under solvent-free conditions. Compared to the classical Biginelli reaction conditions, the present method has the advantages of giving good yields, short reaction times, near room temperature conditions and the ...
Nano-SbCl5.SiO2 and SbCl5.SiO2 are bench-top catalysts which are reusable, readily available, versatile andefficient for promotion of many acid catalyzed organic reactions. These catalysts do not need specialprecautions for preparation, handling or storage, and they can be stored at an ambient temperature for monthswithout losing their catalytic activity. 4-dihydropyrimidin-2(1H)-ones(thiones) ...
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