نتایج جستجو برای: x ray diffraction and ftir

تعداد نتایج: 16938614  

2014
Manjusha Hariharan Benny Cherian

Calcium carbonate nano particles were synthesized using precipitation method from cockle shells by employing chitosan as precursor. Synthesized Calcium carbonates were characterized using scanning electron microscopy (SEM), X-ray diffraction (XRD), UV-Visible and FTIR Spectroscopy. The results were compared with commercial calcium carbonate nano particles. Cockle shells are the potential source...

In the present study, the structural, optical and thermal behaviors of GeO2-PbO-CaO-SrO glasses were investigated to achieve the highest optical properties and thermal stability. Accordingly, different 50GeO2-(50-x)PbO-xCaO and 50GeO2-(50-x)PbO-xSrO (x=0, 10, 20) germanate glasses were prepared by the conventional melt and quench technique between two steel sheets. The produced samples were cha...

بهمنش, اسماء, حسن‌پور, احمد, نیایی‌فر, محمد,

Praseodymium ion (Pr3+) substituted yttrium iron garnet nanoparticles PrxY3-xFe5O12 (x = 0.0, 0.1, 0.2, 0.3, 0.4) were fabricated by the sol-gel method. X-ray diffraction (XRD) patterns confirmed the pure garnet structure for all samples. The chemical bonds and the garnet phase were studied by using Far-FTIR. The magnetic hyperfine parameters were obtained by MÖssbauer spectroscopy and confirme...

درودیان, مسعود, طیبی فرد, سید علی , یزدانی راد, رحیم, احمدی, کامران,

X-ray powder diffraction data for Mo2.85Al1.91Si4.81 are presented here. The new Mo2.85Al1.91Si4.81 compound was successfully prepared, using the self-propagating high-temperature synthesis (SHS) technique. The starting atomic mixture of reactant powders was Mo + 2(1 - x)Si + 2xAl with 0.2 ≤ x ≤ 0.5. The final powder compound obtained by the SHS technique was determined to be in x = 0.2; Mo(Si,...

In this research zinc oxide (ZnO) nano-crystalline powders were prepared by sol-gel method using zinc acetate. The ZnO nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), ultraviolet-visible (UV-Vis), Fourier transform infra-red (FT-IR) and energy dispersive X-ray (EDX) spectroscopy. The structure of nanoparticles was studied using XRD pattern. The c...

A green, efficient and selective approach for the oxidation of sulfides to sulfoxides and sulfones with UHP at room temperature is reported. The reaction is performed in the presence of vanadia catalyst supported on mesocellular silica foam (MCF) with a V content ranging from 2% to 10% as heterogeneous and reusable catalyst. The structural and textural characterization of this catalyst were don...

M. Ghomi Gilvaee M. R. Khanlary, S. Ghammamy

In this research Calcium fluoride nanoparticles and its different amount of cerium ion dopant (5%and 10%) were prepared. The mentioned nanoparticle were studied by fourier transform infrared spectroscopy (FTIR) , X-ray diffraction (XRD), absorption and photoluminescence spectra (PL) and Scanning electron microscopy (SEM). The XRD patterns indicate a typical cubic fluorite structure and no other...

Journal: :journal of physical & theoretical chemistry 2010
zahra sharafi

the x-ray charge density analysis of a hydroxynaphthoquinnne derivative was obtained by multipolar hansen-coppens formalism refinement through high resolution x-ray diffraction data at 100(1) k. the molecularproperties of the title compound resulted from the combined experimental and the quantum theory of atoms inmolecules (qtaim) studies. the topological properties of the covalent bonds and of...

Journal: :journal of nanostructures 2015
b. f. mirjalili a. bamoniri s. m. nezamalhosseini

the knoevenagel condensation of aromatic aldehydes with barbituric acid, dimedone and malononitrile occurred in the presence of bf3/nano-γ-al2o3 at room temperature in ethanol. this catalyst is characterized by powder x-ray diffraction (xrd), fourier transform infrared spectroscopy (ft-ir), thermal gravimetric analysis (tga), field emission scanning electron microscopy (fesem) and energy-disper...

F. Bustanafruz M. Fazli M. Jafar-Tafreshi,

Aluminum sulfate nano structures have been prepared by solution combustion synthesis using aluminum nitrate nonahydrate (Al(NO3)3.9H2O) and ammonium sulfate ((NH4)2SO4). The resultant aluminum sulfate nano structures were calcined at different temperatures to study thermal  decomposition of aluminum sulfate. The crystallinity and phase of  the as-synthesized and calcined samples were char...

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