We present a new method of growing pure solid hydrogen peroxide in an ultra high vacuum environment and apply it to determine thermal stability of the dihydrate compound that forms when water and hydrogen peroxide are mixed at low temperatures. Using infrared spectroscopy and thermogravimetric analysis, we quantified the isothermal decomposition of the metastable dihydrate at 151.6 K. This deco...

A polar fraction obtained from banana fruit pulp by high-vacuum distillation / solvent extraction (pentane-dichloromethane, 2 + 1) and subsequent liquid chromatography on silica gel was derivatized with isopropylisocyanate. Separation of enantiomers of heptan-2-ol and Z-4-hepten-2-ol was performed via their carbamates by means of multidimensional gas chromatography using an achiral (D B -5, col...

We construct new entanglement distillation protocols by interpolating between the recurrence and hashing protocols. This leads to asymptotic two-way distillation protocols, resulting in an improvement of the distillation rate for all mixed Bell diagonal entangled states, even for the ones with very high fidelity. We also present a method how entanglement-assisted distillation protocols can be c...

Distillation is an essential separation process in the chemical and petrochemical industry. The distillation process is a highly nonlinear, complex, interactive and non -stationary, therefore its control is difficult. In the present work an adaptive neuro-fuzzy controller is designed to control a binary distillation process. A conventional PID controller is also designed for comparison purpose....

Distillation is a widely used separation method in the process industries and it is the largest energy consumer among individual process units. Improvement of energy efficiency in distillation systems is still an active research field. Among the issues concerned with the improvement of energy efficiency of distillation systems, the optimal design and synthesis A SHORT Note ABOUT ENERGY-EFFICIEN...

The insertion, elimination and isomerisation of octenes with di-n-octylaluminium hydride [HAl(Oct)2], tri-n-octylaluminium [Al(Oct)3] and sec-octylaluminium species have been studied as individual steps in a putative aluminium based contrathermodynamic olefin isomerisation process. While elimination of 1-octene from [Al(Oct)3] is energetically unfavourable, the process is driven by high tempera...

Plants of genus Leucas belongs to family Lamiacae and have been widely employed by the traditional healers to cure many diseases. The objective of the study was to do preliminary phytochemical screening of Ethanolic Extract of Leaves of Leucas indica (EELLI). About 1000 gm of air dried powdered material of leaves of Leucas indica was extracted with 90% ethanol in a soxhlet extractor for 36 hour...

Invariant rectifying and stripping (IRS) curves are used for thermodynamic analysis of a distillation column. Thermal integration of a distillation column with the background process through side exchangers (side reboilers/condensers) is important for energy-efficient design of a distillation column. Thermal integration of a distillation column through side exchangers also improves the exergeti...

medicinal plante borazambol with the scientific name of perovskia abrotanoides karel. belongs to the family lamiaceae. it is growing wild in the margin of mountainous roads of arid and cold climate of north iran. it is for a long time that indigenous people by different methods in traditional medicine use its products in preventing and curing diseases. in this research, essential oils of perovs...

This paper is concerned with the computer-aided optimal design of reaction-distillation processes. The production of solvent 2,3-dimethylbutene-1 by isomerization of 2,3dimethylbutene-2 is considered as an innovative benchmark problem. Possible process candidates are a reactive distillation column, a reactor coupled to a nonreactive distillation column or a reactive reboiler with a nonreactive ...