Bi2Mn2O7 nano-powders were synthesized via a stoichiometric 1:1 Bi:Mn molar ratio hydrothermal method at 180 °C for 48 h in a 1M NaOH aqueous solution; and solid state method, using Bi(NO3)3.5H2O and MnO2 as raw materials. The synthesized materials were characterized by powder X-ray diffraction (PXRD) technique. Also, the rietveld analysis was done in FullProf in profile matching mode. It was f...

sol-gel derived sulfur modified and pure zno nanorod were prepared using zinc chloride and thiocarbamide as raw materials. prepared nanorods were characterized by means of x-ray diffraction (xrd), thermogravimetry- differential scanning calorimetry (tg–dsc), uv- vis absorption spectroscopy, brunauer emmett teller (bet) specific surface area and barrett joyner halenda (bjh) pore size distributio...

Nano-structure of Co–Mn spinel oxide was prepared by thermal decomposition method using [Co(NH3)4CO3]MnO4 as the precursor. The properties of the synthesized material were characterized by X-Ray Diffraction (XRD), Brunauer-Emmett-Teller (BET), Transmission Electron Microscopy (TEM), surface area measurements, Energy-Dispersive X-ray (EDX) spectroscopy analys...

In this investigation, the selected activated carbon is treated in NaOH solution or gas fluid with ozone from an ozone generator. FTIR, BET specific surface area and element analysis instruments were used to identify the difference in the chemical and physical characteristics between the activated carbon and oxidized activated carbon. The system of adsorption apparatus consists of a fixed adsor...

Amino-functionalised metal-organic frameworks UiO-66 and -67 were post-synthetically modified with salicylaldehyde. A molybdenum complex was immobilised on the resulting materials. They were characterised by (13)C-MAS-NMR, XPS and PXRD to confirm immobilisation and stability. The immobilised complex is an active and reusable catalyst for olefin epoxidation with tert-butyl hydroperoxide (TBHP) a...

nanostructured iron oxide powder that has been recovered from waste pickling liquor unit of steel industry was studied for oxidation catalytic applications. in this research, the powder was characterized by x-ray diffraction (xrd) and transition electron microscopy (tem) for determination of phase structure, morphology and particle size. furthermore, the specific surface area of the powder was ...

Porous (Zr0.5,Sr0.5)TiO3 and MgO (1, 3, 5 mol%) doped ZST nanocomposites have been developed and investigated as humidity sensing elements. The surface area analyser and FESEM data have indicated that the MgO doped perovskites are contained of the macropores and grain size of about 77 to 87 nm. EFTEM proved the reduction of particle size by addition of MgO dopant concentration. While pure ZST s...

Volumetric N 2 adsorption at ?196°C is generally accepted as “gold standard” for estimating the Brunauer-Emmet-Teller (BET) surface area of nanocellulose. It unclear however, whether BET nanocellulose obtained such low temperatures and pressures meaningful an absolute sense, used ambient temperature pressure. In this work, a systematic evaluation using highly crystalline bacterial cellulose (BC...

A method for measurement of dimensions of platy particles of exfoliating, or delaminating, materials, such as clays, in aqueous suspensions in situ is proposed. Equivalent spherical diameter (esd), measured by many common methods, depends more on the major (lateral) dimension of a particle, while it is less sensitive to changes of the particle thickness. Addition of the second method, results o...