A novel graphene-based voltammetric immunosensor for sensitive detection of okadaic acid (OA) was developed. A simple and efficient electrografting method was utilized to functionalize graphene-modified screen-printed carbon electrodes (GSPE) by the electrochemical reduction of in situ generated 4-carboxyphenyl diazonium salt in acidic aqueous solution. Next, the okadaic acid antibody was coval...

Background: This research was focused on the development of a quick, simple, precise, and cost-effective voltammetric method for quantifying dosulepin. Materials Methods: The antidepressant drug (dosulepin) assessed in pharmaceutical formulations using square wave (SWV) Differential pulse (DPV) techniques at glassy carbon potentiometric working electrodes (GCE). Results: Dosulepin demonstrated ...

A new dimeric Cu(II) complex [Cu(mu(2)-hep)(hep-H)](2).2PF(6) (1) containing a bidentate (hep-H = 2-(2-hydroxyethyl)pyridine) ligand was synthesized and characterized by single crystal X-ray diffraction studies. Each Cu ion in 1 is in a distorted square pyramidal geometry. Further 1 is used as a modifier in the construction of a biomimetic sensor for determining phenols [phenol (Phe), resorcino...

The electronic and electron transfer behaviour of two examples of a recently discovered class of triple-decker sandwich complex based on three phthalocyanine ligands linked by two chelated cadmium ions has been investigated by EPR spectroscopy and cyclic voltammetry, square wave voltammetry and linear sweep voltammetry experiments. The two compounds, and , differ in the location of the eight al...

تم تطوير طريقة التحليل الكهربائي الانتقائية والحساس لتحديد الرصاص عن طريق قياس الجهد بالموجة المربعة (SWV)في وجود حمض البيريدين -3 الكربوكسيل (حمض النيكوتين ، NA). يتراكم معقد Pb-NA على سطح قطب زئبقي محكوم النمو (GCME)ويقاس تيار الذروة بواسطة الفولتميتر (SWV) يتم تقليل المعقد وزيادة التيار بمقدار 1.5 مرة عند إضافة النيكوتينيك إلى محلول العينة.تم تقييم الظروف الكيميائية والفيزيائية التي كتنت افض...