Solid dispersions of tanshinone IIA (TanIIA) using hydroxyapatite (HAp) as the dispersing carrier (TanIIA-HAp SDs) were prepared by the solvent evaporation method. The formed solid dispersions were characterized by scanning electron microscopy (SEM), differential scanning calorimetry analysis (DSC), X-ray powder diffraction (XRPD) and Fourier transforms infrared (FTIR) spectroscopy. The in vitr...

New forms of vanadium oxide Nanoporous were fabricated using a simple chemical synthesis method. Vanadium pentoxide (V2O5) Nanoporous were synthesized by sodium metavanadate as precursor and ethylene glycol as surfactant. The samples were characterized by high resolution transmission electron microscopy (HRTEM), field effect scanning electron microscopy (FESEM) and X-ray diffraction (XRD), Four...

in this research, cobalt and nickel sulfide nanoparticles (nps) were grown on almcm-41 matrix by using ion exchange method. the prepared samples were irradiated by thermalized neutron that emitted from am-be source up to fluencies (7.9+e9n/cm2). after that, x-ray diffraction (xrd), uv-vis spectroscopy, fourier transform infrared (ftir), scanning electron microscopy (sem) and transmission electr...

in this paper we report an eco-friendly route for the synthesis of sliver nanoparticles using agaricus bisporus (white button mushroom) extract. the synthesized silver nanoparticles were confirmed and characterized by uv-visible spectrum of the aqueous solution containing silver ions showed a peak at 420 nm corresponding to the surface plasmon absorbance of silver nanoparticles. transmission el...

Nanoparticles of titanium dioxide doped with Fe2+ ions have been synthesized via sol-gel technique using Titanium tetraisopropoxide (TTIP) and ferrous sulphate as a precursors. The synthesized nanopowders were characterized by Powder X-ray Diffraction (PXRD), Scanning Electron Microscope (SEM), Fourier Transform Infrared (FTIR), Ultraviolet Visible (UV-Vis) and Photoluminescence (PL) Spectrosco...

In the Present work structural, morphological and compositional properties of ZnO nanopowders synthesized using Zinc nitrate and NaOH using sol-gel process were reported. The synthesized nanopowders were further analyzed using X-Ray Diffraction (XRD), Scanning electron microscopy (SEM) and Fourier Transform Infrared (FTIR) spectroscopic characterizations. Crystalline size and Lattice strain det...

Polypyrrole–hydroxyethylcellulose/TitaniumDioxide (PPy-HEC/TiO2) nanocomposite was synthesized via in situ chemical oxidative polymerization method at room temperature in water and water/ethyl acetate solution in the presence of ferric chloride (FeCl3). The effect of TiO2 nanoparticles and HEC on the characteristics of products such as thermal stability and morphology was investigated. The fabr...

In the present investigation, Bambusa bambos was used for optimization of enzymatic pretreatment and saccharification. Maximum enzymatic delignification achieved was 84%, after 8 h of incubation time. Highest reducing sugar yield from enzyme-pretreated Bambusa bambos was 818.01 mg/g dry substrate after 8 h of incubation time at a low cellulase loading (endoglucanase, β-glucosidase, exoglucanase...

Aromatic bis-aldehydes have been used as building blocks in the synthesis of polyazomethines (a class of conjugated Schiff bases) and their physicochemical properties have been studied. Six dialdehydes have been synthesized, 3a-3f, via etherification reaction between aromatic diols (2a-2f) and 4-fluorobenzaldehyde (1) (see Scheme 1), and then polymerized with 1,4-phenylenediamine (4a) and 4,4'-...

Sugarcane bagasse was delignified with alkali and peracetic acid in a two-stage process to obtain pulps with high yield and low kappa number. The experimental results indicated that alkali pretreatment prior to peracetic acid (PAA) delignification could significantly reduce PAA loading by partially removing lignin and swelling the fibers. An optimum condition for the two-stage delignification w...