نتایج جستجو برای: nh2 sba 15

تعداد نتایج: 505221  

2015
Qilu Yao Zhang-Hui Lu Kangkang Yang Xiangshu Chen Meihua Zhu

Ultrafine ruthenium nanoparticles (NPs) within the mesopores of the SBA-15 have been successfully prepared by using a "double solvents" method, in which n-hexane is used as a hydrophobic solvent and RuCl3 aqueous solution is used as a hydrophilic solvent. After the impregnation and reduction processes, the samples were characterized by XRD, TEM, EDX, XPS, N2 adsorption-desorption, and ICP techn...

پایان نامه :وزارت علوم، تحقیقات و فناوری - دانشگاه بیرجند - دانشکده علوم پایه 1391

چکیده: در این کار پژوهشی کمپلکس های [fe(bpdo)2cl2]cl (2 و?2 بی پیریدین n و n? دی اکسید = bpdo) و [fe(bpy)2cl2]cl )2 و?2 بی پیریدین =bpy (سنتز و با روش اشباع سازی در نانو بستر al-sba-15 تثبیت شدند. این نانو کاتالیزور ها به وسیله تکنیک های xrd، tem، bet (جذب – واجذب نیتروژن(، ft-ir و آنالیز عنصری شناسایی شدند. الگوی xrd و آنالیز tem مربوط به[fe(bpdo)2cl2]cl/al-sba-15 و [fe(bpy)2cl2]cl/al-sba-1...

Journal: :Dalton transactions 2015
Yolanda Pérez Isabel del Hierro Lydia Zazo Rafael Fernández-Galán Mariano Fajardo

A family of heterogeneous catalysts has been prepared by employing different strategies: firstly by direct reaction or grafting of titanium, zinc, aluminium and magnesium precursors with dehydrated SBA-15 and secondly by reaction of the metallic derivatives with a hybrid SBA-15 mesoporous material, which possesses a new covalently bonded linker based on an amino alcohol chelate ligand. These ma...

Journal: :iranian journal of chemistry and chemical engineering (ijcce) 2015
hamid reza pouretedal sara basati

grinding (solvent-free) method was used as a superior technique to prepare mesoporous photocatalysts of zno, zns, zno / zns, cdo, cds and cdo / cds-sba-15. in this technique, the nitrate, acetate and chloride salts of zinc and/or cadmium were grinded with as-synthesized sba-15 as a mesoporous material. the controllable sulfurationis was used to prepare zns, zno/zns, cds and cdo/cds-sba-15 at te...

Journal: :Solid state nuclear magnetic resonance 2009
Jörg Frey Yean Sang Ooi Bejoy Thomas V R Reddy Marthala Arne Bressel Thomas Schölkopf Thomas Schleid Michael Hunger

SBA-15 was utilized as mesoporous support for the dispersion of vanadium phosphate (VPO) compounds. Loading of SBA-15 with VPO compounds was found to be accompanied by decreasing (29)Si MAS NMR signals of Q(2) (Si(2Si,2OH)) and Q(3) (Si(3Si,1OH)) silicon species, which indicates coverage of the mesoporous support by the guest compounds. The (51)V MAS NNR spectra of the activated VPO/SBA-15 cata...

2017
Alina Stefanache Maria Ignat Catalina A. Peptu Alina Diaconu Iulian Stoleriu Lacramioara Ochiuz

Magnolol (MG) is a small-molecule neolignan polyphenolic compound isolated from the genus Magnolia. The anti-inflammatory, anti-oxidative, anti-diabetic, anti-tumorgenic, anti-neurodegenerative, anti-depressant and anti-microbial properties of MG are well documented in recent literature. These fascinating multiple biological activities of MG encourage research about the development of new deliv...

Hamid Reza Pouretedal, Sara Basati

Grinding (solvent-free) method was used as a superior technique to prepare mesoporous photocatalysts of ZnO, ZnS, ZnO / ZnS, CdO, CdS and CdO / CdS-SBA-15. In this technique, the nitrate, acetate and chloride salts of zinc and/or cadmium were grinded with as-synthesized SBA-15 as a mesoporous material. The controllable sulfurationis was used to prepare ZnS, ZnO/ZnS, CdS and CdO/CdS-SBA-15 a...

Journal: :Bioresources 2023

The stable silica sieve-based HBeta-SBA-15 catalyst-carrier was successfully prepared by a hydrothermal synthesis method, and then Ni2P/HBeta-SBA-15 new hydrodeoxygenation catalyst loaded the equal volume impregnation method. It characterized X-ray diffraction (XRD), N2 adsorption-desorption, scanning electron microscopy (SEM), transmission (TEM), pyrolysis-infrared (Py-IR) methods. results sho...

A carrier system based on nanoporous silica (SBA-15) with magnetic nanoparticles of CoFe2O4 was synthesized via the impregnation of cobalt salt, iron salt and citric acid with as-synthesized SBA-15. The obtained samples were characterized by small angle X-ray scattering (SAXS), N2 adsorption/desorption, scanning electron microscopy (SEM), vibrating sample magnetometer (VSM) and ultraviolet (UV)...

Hamid Reza Pouretedal Sara Basati

Mesoporous photocatalysts of CeO2/SBA-15 are prepared by two methods of direct synthesis as solvent-usage and solvent-free methods. In solvent-usage method, CeO2/SBA-15 is synthesized in acidic media. While, in solvent-free method, CeO2/SBA-15, has been prepared through the novel path of directly grind cerium salt into the as-prepared samples of SBA-15 occluded ...

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