А para-chlorophenyl substituent was firstly obtained into the structure of pyridyl-substituted 4-nitrosopyrazole by cyclocondensation hydrazine hydrate with corresponding isonitroso-β-dicarbonyl compounds. The previously unknown 3(5)-(4-chlorophenyl)-5(3)-pyridine-(3(4))-yl-4-nitroso-1H-pyrazoles and 3(5)-alkyl(aryl)-5(3)-pyridine-(3(4))-yl-4-nitroso-1H-pyrazoles is proved studied in detail mod...

In natural gas exploitation, foam drainage, corrosion inhibition and hydrate of wellbore fluid are conventional operations. However, there is often a problem where multiple chemical agents cannot be effectively used together can only separately, resulting in complex production processes. this study, the final integrated formulation was determined: 0.1% sodium alpha-olefin sulfonate (AOST) + 0.3...

Fe2O3 nanoparticles (NPs) with mean size of 50 nm ca. are synthesized starting from a porous organic polymer containing β-ketoesterate Fe(III) sites (Fe-POP), which is annealed at 400 °C under air for 30 min. During calcination, the material partially decomposes, and iron(III) oxide NPs onto an residue could be observed after annealing. The obtained characterized by SEM-EDS, IR, magnetic analys...

High-surface-area, nitrogen-doped carbon microflowers (A-NCFs-4) assembled from porous nanosheets are prepared in a three-step process: soft-templating self-assembly, thermal decomposition, and KOH activation. The hydrazine hydrate used in our experiment serves not only as a structure-directing agent, but also as a nitrogen source. The resultant A-NCFs-4 has a hierarchical porous structure and ...

In the present work, interaction of the strategic starting material, methyl 2-isothiocyanatobenzoate (1), with sulfa drugs resulted in the formation of methyl 2-[3-(4-(N-substituted sulfamoyl)phenyl)thioureido] benzoates 2-5, which upon reaction with hydrazine hydrate afforded N-amino derivatives 6-9. Triazoloquinazoline derivatives 10-18 were obtained via reaction of compounds 6-8 with aromati...

Different morphologies of Ag2Te nanostructures were synthesized using TeCl4 as a new precursor and hydrazine hydrate as reducing agent by a hydrothermal method. Various parameters that affect on morphology and purity of nanostructures were optimized. According to our experiments the best time and temperature for preparation of this nanostructure are 12 h and 120 °C. The photo-catalytic behaviou...

In the present work we describe the structure and the spectroscopic characterization of a spirocyclic derivative of a rhodamine B ligand whose properties allow discrimination of light-up effects induced by metal ion chelation and variation of pH. Distinction of the two effects is important for the use of this type of ligand to detect and monitor metal ions in aqueous solutions. The synthesis of...

Nanocrystalline semiconducting thin films of copper sulphide (Cu2S) were deposited by novel chemical route using aqueous solution of 0.1 M copper chloride, 0.05 M thiourea, complexing agent 10% aqueous ammonia (NH3) and hydrazine hydrate. The characterization and gas sensitivity of as deposited Cu2S thin film sensor have been investigated. The as deposited Cu2S thin films were observed to be ve...

BACKGROUND Various methods are available to measure serum cholesterol concentrations. Of these, the cholesterol ester hydrolase (CEH)-cholesterol oxidase-peroxidase chromogenic method is widely used. However, this method has the disadvantage of interference by reducing substances. We developed and evaluated an endpoint assay for serum cholesterol, based on a CEH-cholesterol dehydrogenase (CDH)-...