Currently, high crystalline quality materials such as carbon nanotubes (CNTs) are produced only at a temperature in an excess of 500 C. This paper reports on low-temperature synthesis of CNTs by selective heating of catalytic particles using two complementary mechanisms: enhanced exothermic catalytic reactions and inductive heating by radio frequency electromagnetic fields.

Benzylation of alcohols and other substrates under thermal conditions translates smoothly from conventional heating into MW-assisted organic synthesis (MAOS). Reactions times are decreased from hours to minutes while good to excellent yields are maintained. MW heating should be considered for benzylation of high-value substrates using the title reagent.

As the range of techniques for microwave heating has expanded, so have the areas in which it can have a profound impact. Two emerging areas are the application of microwave heating for the synthesis of peptides, peptoids, oligopeptides and carbohydrates and in the field of proteomics.

A direct synthesis of substituted xanthenes from salicylaldehydes and cyclohexenones or tetralones has been developed. The reaction is catalysed by Lewis acids like scandium triflate and furnishes substituted xanthenes in good to excellent yields using either microwave or thermal heating. Microwave heating results in significantly shortened reaction times of 30 min and generally higher yields.

This study focuses on an aqueous one-pot method for synthesis of CdSe/ZnS core/shell QDs using microwave radiation. The novelty of the study is the use of Zn(NH3)4 as the zinc source. Using an initial solution with the composition Cd1Se1Zn6MPA20, the QDs obtained upon heating at 160 °C for 60 min were not high quality, as evidenced by a quantum yield of 1.5%, due to the poor interface between t...

During heat treatment, the work piece experiences a range of heating rates depending upon the sizes and types of furnace. When the Al-Si-Mg cast alloy is heated to the solutionizing temperature , recrystallization takes place during the ramp-up stage. The effect of heating rate on recrystallization in the A356 (Al-Si-Mg) alloy was studied using dilatometric and calorimetric methods. Recrystalli...

Approximate analytical and full numerical solutions are obtained for the transient response of both a pure water and solution droplets to both short- and long-time laser heating. The differences in the temperature and size histories between pure water and solution droplets are elucidated. The validity of of the approximate analytical solution, extended from that of Armstrong ["Aerosol Heating a...