Abstract Two-dimensional gas chromatography coupled to time-of-flight mass spectrometry (GC × GC-TOFMS) is a powerful tool for identification of compounds in complex samples. Herein, we compared the GC GC-TOFMS and systems polar metabolite profiling rice seeds. Forty-seven thirty-six metabolites were detected Korean cultivar, Dongjin, using GC-TOFMS, respectively. The limits detection shikimic,...

In this study, a simple and reliable method by gas chromatograph–mass spectrometry (GC–MS) was developed for the fast and regular identification of 3, 4-MDMA impurities in ecstasy tablets. In so doing, 8 samples of impurities were extracted by diethyl ether under alkaline condition and then analyzed by GC–MS. The results revealed high MDMA levels ranging from 37.6% to 57.7%. The GC-MS method sh...

Different solvent extracts of a red algae, Hypnea flagelliformis,and two brown algae, Cystoseira myrica and Sargassum boveanum, collected from the Persian Gulf coast were subjected to different bioassays including: 1,1-diphenyl-2-picrylhydrazyl (DPPH) free radical scavenging assay, antibacterial and antifungal activity by thin layer chromatography (TLC)-bioautography, agar disc diffusion (ADD) ...

The present study presents the bioactive profile of Polygala arillata Buch.-Ham ex D.Don using GC-MS. The phytochemical constituents of leaf and stem ethanolic extracts of Polygala arillata were investigated using Fisons Gas-chromatography – Mass spectrometry. The mass spectra of the compounds in the leaf and stem extracts was matched with National Institute of standards and Technology (NIST) L...

Mass spectrometry coupled to gas chromatography (GC-MS) has been widely applied in the field of metabolomics. Success of this application has benefited greatly from computational workflows that process the complex raw mass spectrometry data and extract the qualitative and quantitative information of metabolites. Among the computational algorithms within a workflow, deconvolution is critical sin...

This review aims at summarizing the most recent updates in the field of acrylamide (AA) formation (mechanism, conditions) and the determination of AA in a number of foods (fried or baked potatoes, chips, coffee, bread, etc). The methods applied for AA detection [Capillary Electrophoresis-Mass Spectrometry (CE-MS), Liquid Chromatography-Mass Spectrometry (LC-MS), Non-Aqueous Capillary Electropho...

Fast and reliable analytical methods for mercury speciation would aid in understanding mercury offgas chemistry. Presently, the U.S. Environmental Protection Agency (EPA) regulates only total mercury; however, many studies indicate that mercury toxicity is highly dependent on the mercury speciation. For example, amalgams and mercury sulfides have relatively low toxicities, while organomercury a...

A gas chromatograph/electron capture detector-ion trap mass spectrometer (GC/ECD-ITMS) was used for the determination of polybrominated diphenyl ethers (PBDEs) in euryhaline fish and crabs. GC/ECD-ITMS results showed that average recoveries from the spiked fish samples are in a range of 58-123% with relative standard deviations (RSDs) of 5-19%. PBDE concentrations obtained from GC/ECD-ITMS rang...