In this research, the characteristics of CMP dioxane lignin (hardwood origin) and soda bagasse lignin (ethanol soluble fraction) and dioxane lignin of bagasse were studied using gel permeation chromatography, gas chromatography-mass spectrometry and 13C NMR spectroscopy and DFRC degradation procedure. The results indicated that the main structural units in lignins are phenyl propane skeletons b...

In this report, the degradation of 1-Naphthol was studied under xenon irradiation for 2 h using    WO3-rGO nanocomposite as photocatalyst. Raman spectroscopy and scanning electron microscopy demonstrated nanocomposite formation. Gas chromatography-mass spectrometry (GC-MS) technique which was utilized to analyze the degradation products, confirmed the formation of salicylic acid as a...

a fiber coating from polyaniline (pani) was electrochemically prepared and employed for solid phase micreoextraction (spme). the pani film was directly electrodeposited on the platinum wire surface using cyclic voltametry (cv) technique. the same method was applied for the preparation of spme fiber coated by polyaniline multiwalled carbon nanotubes (pani/mwcnts) composite. the concentration of ...

this study propose a new analytical protocol for the determination of benzene, xylene, toluene and styrene in water samples using homogeneous liquid-liquid microextraction via flotation assistance (hllme-fa) technique followed by gas chromatography-mass spectrometry (gc-ms). in this research, a special extraction cell was designed to facilitate collection of the low-density solvent extraction. ...

Derivatization reactions are meant to transform an analyte for detectability in Gas Chromatography (GC) or other instrumental analytical methods. Derivatization in GC analysis can be defined as a procedural technique that primarily modifies an analyte’s functionality in order to enable chromatographic separations. A modified analyte in this case will be the product, which is known as the deriva...

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Relative to other metabolomics analysis techniques, gas chromatography mass spectrometry (GC/MS) is one of the earliest applied analysis techniques in metabolomics. The first paper on metabolomics (metabolic profiling) is derived from the application of GC/MS analysis in urine and tissue extracts (Dalgliesh et al. 1966). With the arrival of omics era and the proposing of metabolomics concept, p...

RECEIVED for review February 21, 1978. Accepted June 19, 1978. NMR spectra since two distinct peaks (6 -3.38, 3.78 ppm) caused by these protons are observed in CDCA vs. only one peak (6 -3.45 ppm) caused by the same protons in UDCA. T h e fingerprint region of the spectrum (6 1-2.5 ppm) and the relative position of the CIS methyl peak with respect to tha t of the doublet caused by the Cpl methy...

Gas chromatography coupled to mass spectrometry in negative chemical ionization (NCI) 11 mode has been applied to the quantification and reliable identification of polybrominated 12 diphenyl ethers (PBDEs) in animal and vegetable samples from aquaculture activities. 13 Matrices analyzed included fish fillet, fish feed, fish oil and linseed oil, which their fat content 14 ranged from 5 to 100%. ...