One-step mid- and far-Fourier-transform (FT)-IR spectroscopy is a facile powerful tool that provides various information regarding chemical crystal states. However, its potentially high applicability has not been sufficiently demonstrated. In the present study, ibuprofen (IB)-loaded MgO samples are prepared via different methods, they evaluated using scanning electron microscopy (SEM), thermogr...

easily prepared nanozno was found to be as an efficient catalyst in the synthesis of 1,4-dhps via four-component reaction of 1,3-dicarbonyls, aldehydes and ammonium carbonate in water at 60 °c. the prepared nanozno was characterized by xrd and ft-ir analysis, while the determined specific surface area of nano catalyst by bet method was 33 m2/g.

the knoevenagel condensation of aromatic aldehydes with barbituric acid, dimedone and malononitrile occurred in the presence of bf3/nano-γ-al2o3 at room temperature in ethanol. this catalyst is characterized by powder x-ray diffraction (xrd), fourier transform infrared spectroscopy (ft-ir), thermal gravimetric analysis (tga), field emission scanning electron microscopy (fesem) and energy-disper...

Instrumentation is described that has been constructed at the National Institute of Standards and Technology (NIST) for the measurement of regular re ̄ectance and transmittance over the 2±25 mm wavelength region. This includes both specialized accessories used with Fourier-transform infrared (FT-IR) spectrometers and laser-based systems for high optical density transmittance measurements. The FT...

The aim of this paper is to know the compositions in unknown medicinal-lotion and to evolution its applications. Through a variety of studies, an analysis method was established. This method mainly is that samples were first extracted and pre-treated by concentration of compositions, and then they were separated and qualitatively analyzed by multiple-instruments. These instruments involve Mass ...

In this paper, a new photocoinitiator for free radical photopolymerization, belonging to the benzodioxole (BDO) derivatives, was synthesized and characterized, and the effect of phenyl at the 2-position of BDO was estimated. The structure of PhBDO was characterized by elemental analysis, (1)H NMR and (13)C NMR. Laser flash photolysis (LFP) and an electron spin resonance spin trapping technique ...

The authenticity of milk and milk products is important and has extended health, cultural, and financial implications. Current analytical methods for the detection of milk adulteration are slow, laborious, and therefore impractical for use in routine milk screening by the dairy industry. Fourier transform infrared (FT-IR) spectroscopy is a rapid biochemical fingerprinting technique that could b...

Different yew species contain poisonous taxane alkaloids which serve as resources for semi-synthesis of anticancer drugs. The highly variable amounts of taxanes demand new methods for fast characterization of the raw plant material and the isolation of the target structures during phyto extraction. For that purpose, applicability of different vibrational spectroscopy methods in goods receipt of...