Uma série de cetonas e ésteres α,β-insaturados β-amino ésteres, 4a-h e 6a-d, derivados de α-amino ácidos foi obtida a partir dos cloridratos dos α-amino ésteres 2a-d e dos compostos 1,3-dicarbonílicos 3a,b e 5 em presença de trietilamina. Estes compostos foram preparados empregando energia de microondas, sem uso de solvente, utilizando como suporte sólido K-10 ou KSF e também foram efetuadas re...

Diversity-oriented synthesis (DOS) is an important field involving the synthesis of libraries of diverse small molecules for applications including biological screening. The last decade has witnessed major progress in the field, with continued emphasis on structural and functional diversity for DOS library construction. A number of recent reviews have updated the community on this topic, includ...

1DDS, MSc, PhD, Graduate Student (PhD degree), Department of Dental Materials and Prosthodontics, UNESP – São Paulo State University “Júlio de Mesquita Filho” São José dos Campos Dental School. 2DDS, MSc, PhD, Associate Professor, Department of Dental Materials and Prosthodontics, UNESP – São Paulo State University “Júlio de Mesquita Filho” São José dos Campos Dental School. 3DDS, MSc, PhD, Ass...

The partial occupation numbers and density of states (DOS), and the total DOS at the Fermi level are calculated as a function of reduced atomic volume for bcc and fcc alkali metals employing the linearmuffin-tin-orbital (LMTO) method. By means of the abrupt changes obtained in the partial and total DOS values at the Fermi level, good agreement with regard to experiment were found in predicting ...

Availability requires that computer systems function normally without loss of resources to legitimate users. One of the most challenging issues to availability is the denial-ofservice (DoS) attack. DoS attacks constitute one of the major threats and among the hardest security problems in today’s Internet. The main aim of a DoS is the disruption of services by attempting to limit access to a mac...

To clarify the genetic relationships among the Lidia breed lineages and two main Portuguese Lidia bovine populations, Casta Portuguesa and Brava dos Açores, 24 autosomal microsatellites were analyzed in 120 samples. Brava dos Açores showed the highest observed and expected heterozygosity (0.73 and 0.70, respectively) while Casta Portuguesa showed the lowest observed and expected heterozygosity ...

Aminoglycoside antibiotics represent a classical group of antimicrobials first discovered in the 1940s. Due to their ototoxic and nephrotoxic side effects, they are typically only used against Gram negative bacteria which have become resistant to other therapeutics. One family of aminoglycosides includes such compounds as butirosin, ribostamycin, neomycin, and kanamycin, amongst others. The com...

Denial of service (DoS) attacks can be defined as any third-party action aiming to reduce or eliminate a network’s capability to perform its expected functions. Although there are several standard techniques in traditional computing that mitigate the impact of some of the most common DoS attacks, this still remains a very important open problem to the network security community. DoS attacks are...

A semi-analytical extraction method of interface and bulk density of states (DOS) is proposed by using the low-frequency capacitance-voltage characteristics and current-voltage characteristics of indium zinc oxide thin-film transistors (IZO TFTs). In this work, an exponential potential distribution along the depth direction of the active layer is assumed and confirmed by numerical solution of P...

Named Data Networking (NDN) is a promising network architecture being considered as a possible replacement for the current IP-based (host-centric) Internet infrastructure. NDN can overcome the fundamental limitations of the current Internet, in particular, Denial-of-Service (DoS) attacks. However, NDN can be subject to new type of DoS attacks namely Interest flooding attacks and content poisoni...