A non-invasive XRD/XRF instrument for study of works of art has been developed jointly by the Getty Conservation Institute and inXitu Inc. (California). Many aspects of the instrument are based on technologies initially developed for NASA’s planetary XRD/XRF instrument CheMin and used in inXitu’s portable transmission XRD/XRF instrument (Terra). A new geometry was designed based on a reflection...

Thirteen arsenous acid samples of known origins and refining methods were collected. Each sample was subjected to quantitative analysis of any impurity elements present using synchrotron radiation X-ray fluorescence spectrometry (SR-XRF) and inductively coupled plasma-atomic emission spectrometry (ICP-AES). The trace elements selected were Sn, Sb and Bi for the reasons that they were considered...

Micro-X-ray fluorescence (micro-XRF) analysis is a promising method for determining elemental distributions of small regions. Moreover, a recent trend in micro-XRF is 3D elemental analysis by using confocal micro-XRF instruments combined with two polycapillary x-ray lenses. Our research group has been developed confocal micro-XRF instruments by using polycapillary x-ray lenses, and its spatial ...

this article presents the method of extraction-preconcentration of lead, cadmium, and nickel ions from food samples using the ghezeljeh montmorillonite nanoclay (geleh-sar-shoor) as a new native adsorbent in batch single component systems. the extraction-preconcentration of heavy metals were carried out by applying the solid phase extraction (spe) method followed by atomic absorption spectrosco...

The purposes of this study are: (1) to determine whether proficiency analytical test (PAT) materials from the American Industrial Hygiene Association can be used to provide quality data for portable X-ray fluorescence analysis (XRF) of lead in dust wipe surface samples; (2) to provide data to determine whether the on-site analysis of field dust wipe samples by XRF and the laboratory method of i...

Measurements of the refractive index (RI) and elemental analysis using synchrotron radiation X-ray fluorescence spectrometry (SR-XRF) were applied to the forensic discrimination of sheet-glass samples from different origins. The refractive index was calculated from the matching temperature at which the glass fragments became invisible in silicone oil. Fragments smaller than 1 mm in maximum diam...

The essence of adsorbents in water or wastewater treatment cannot be over-estimated. This research paper seeks to investigate the characterisation river sand, beach sand and granite as treatment. River (collected some localities Nigeria) were sieved, washed later sun-dried. These three materials taken laboratory for XRF, SEM EDX analyses. XRF analysis revealed that oxides present selected inclu...