The homogeneity range and crystal structure of the Mg-rich ternary solid solution has been determined using SEM, EPMA/WDS, TEM and X-ray diffraction. This compound has the Ca3MgxZn15 x (4.6 x 12) formula at 335 C. The refinement of the XRD patterns was carried out by Rietveld analysis, XRD data has shown that this solid solution crystallizes in hexagonal structure having P63/mmc (194) space gro...

in this paper, labo3 perovskite type catalyst formulations were prepared by sol-gel auto combustion method using citric acid as the fuel. activity of catalysts was tested in catalytic oxidation of toluene as a model of volatile organic compounds. lacoo3 perovskite formulation showed the highest activity among labo3 (fe, mn and co) perovskite catalysts. so, lacoo3 perovskite based catalyst was s...

TiO2/graphene (TiO2-x/GR) composites, which are Ti(3+) self-doped TiO2 nanorods decorated on boron doped graphene sheets, were synthesized via a simple one-step hydrothermal method using low-cost NaBH4 as both a reducing agent and a boron dopant on graphene. The resulting TiO2 nanorods were about 200 nm in length with exposed (100) and (010) facets. The samples were characterized by X-ray diffr...

caco3 nanoparticles have been synthesized via heat-treatment of a new precursor and solid state reaction. effect of calcinations temperature and quantity of surfactant on particle size has been investigated. the products were characterized by x-ray diffraction (xrd), scanning electron microscopy (sem), transmission electron microscopy (tem) and fourier transform infrared (ft–ir) spectroscopy.

ruthenium dioxide nanoparticles (ruo2 ) with an average particle size of 50 nm are readily synthesized from rucl3.xh2o via the precipitation process in the presence of in-situ sodium octanoate as anionic surfactant. the phase composition, morphology, lattice parameters and size of nanoparticles in these products are characterized by fourier transform infrared spectroscopy (ft-ir), x-ray diffrac...

A technique based on x-ray diffraction (XRD) is introduced to understand the variation of the grain-to-grain ordering in FePt recording media. We classify the possible ways that the grains may be ordered into three types: homogeneous ordering, inhomogeneous ordering, and bipolar ordering. We study the possible impact of each type of ordering on the XRD spectra in terms of the relative angular p...

The structure of GexAs10Se90-x (x=10, 17.5, 22.5, 27.5, 30, 35) glasses as well as some other compositions extensively used in infrared optics, e.g. GASIR® (Ge22As20Se58) and AMTIR-1 (Ge33As12Se55) has been investigated by X-ray diffraction (XRD) and extended X-ray absorption fine structure (EXAFS) measurements at the Ge, As and Se K-edges. Structural models have been obtained by fitting simult...

Epitaxial multilayers and superlattice (SL) structures are gaining increasing importance as they offer the opportunity to create artificial crystals with new functionalities. These crystals deviate from the parent bulk compounds not only in terms of the lattice constants but also in the symmetry classification, which renders calculation of their X-ray diffraction (XRD) patterns tedious. Neverth...

Oxide nanoparticles can exhibit unique physical and chemical properties due to their limited size and a high density of corner or edge surface sites. In this study, MgO nanoparticle was synthesized using Mg(CH3COO)2 and hexamethylenetetramine as starting materials. The structure and optical properties of these particles are investigated by using X-ray diffraction (XRD), sc...

Microwave ferrites require high coercivity for their use as microwave absorbers. Strontium hexaferrite is one of the best material due to its magnetic properties , high coercivity, large unilateral magnetic anisotropy and very low cost in comparison to others make it suitable for the use as microwave components specifically microwave absorber .Strontium nano hexa ferrites were successfully synt...