The inadvertent ingestion of contaminated soil can be an important source of pesticide exposure, especially in young children. The actual level of a pesticide that is available for absorption into a biological system may be much lower than the overall contamination level due to the interaction of each chemical with the solid matrix. This bioaccessibility is dependent on characteristics of the c...

Various traditional systems of medicine enlightened the importance of Pithecellobium dulce. There are reports on the medicinal values of the leaves and seeds of this plant. The present study was discusses the microwave assisted soxhlet extraction of Pithecellobium dulcefruit powder and its screening on pharmacognostical and preliminary phytochemical analysis followed by total phenolic, flavonoi...

Calophyllum brasiliense is a rich source of bioactive coumarins, xanthones and biflavonoids. The aim of the study was to compare the phenol contents and the antioxidant activity of C. brasiliense extracts obtained by conventional and supercritical fluid extraction (SFE) methods, as well as the quantification of crude extracts and (-)-mammea A/BB yields. Dichloromethane and hexane were used as s...

background: blunt abdominal trauma is one of the causes of mortality in emergency department. free fluid in the abdomen due to intra-abdominal blunt trauma can be determined by the surface probe of ultrasound. since the importance of this free fluid in hemodynamic stable patients with blunt trauma is associated with the unknown outcome for surgeons, this study was performed to evaluate the role...

background in stable patients with blunt abdominal trauma, accurate diagnosis of visceral injuries is crucial. objectives to determine whether repeating ultrasound exam will increase the sensitivity of focused abdominal sonography for trauma (fast) through revealing additional free intraperitoneal fluid in patients with blunt abdominal trauma. patients and methods we performed a prospective obs...

The aim of this work was to characterize the initial organic content of a selected municipal solid waste incineration (MSWI) bottom ash. This was realized by elemental carbon analysis using pyroanalysis of untreated samples. In addition, MSWI bottom ash extracts obtained by supercritical fluid extraction (SFE) or hot solvent extraction (Soxtec), were analyzed using gas chromatography (GC) coupl...

Extraction and chromatographic separation of fat-soluble vitamins is a challenging task, due to the sensitivity of these compounds towards light, oxygen, heat and pH. In light of this, supercritical fluid extraction (SFE) and supercritical fluid chromatography (SFC) are attractive techniques as they function at considerably milder conditions than conventional solvent-based analytical techniques...

In this study the first supercritical fluid based protocol for the extraction, analysis, and isolation of six polar compounds, i.e., o-vanillin (1), styracin (2), vanillin (3), trans-cinnamic acid (4), vanillic acid (5), and shikimic acid (6), was developed. First, eight styrax resin products (R1-R8) obtained from various Liquidambar tree species, which are known to contain compounds 2-6, were ...

A method was developed based on supercritical fluid chromatography for quantitative determination of carotenoids in extracts of Scenedesmus sp. By utilizing the low backpressure in supercritical fluid chromatography, a C18 column and a 2-ethyl pyridine column were coupled in series. It was concluded that even minor changes in temperature had a substantial effect on selectivity. A standard mixtu...