Compositions measurement is a vitally critical issue for the modelling and control of distillation process. The product compositions of distillation columns are traditionally measured using indirect techniques via inferring tray compositions from its temperature or by using an online analyser. These techniques were reported as inefficient and relatively slow methods. In this paper, an alternati...

This paper considers the design and control of a reactive distillation column in which one reactant is consumed and two products are formed (A B+C). The volatilities are B ¿ A ¿ C , i.e. the reactant is intermediate boiling between the two products. The metathesis of 2-pentene is considered as the demonstrative example. The column has a single feed of the intermediate boiling reactant. The dist...

Methyl Tert-butyl Ether (MTBE) is an important chemical used as an octane booster in gasoline to replace tetra ethyl lead. Maximum production of the MTBE can be achieved using reactive distillation (RD) process at the optimum operating conditions and column configuration. However, optimizing the column configuration such as tray or catalyst location is experimentally expensive. Therefore, a rel...

Abstract In this work we present a methodology for synthesizing sequences of columns that combine both, the heat integrated and the thermally coupled distillation columns. As a consequence it is possible to design systems capturing simultaneously the advantages of these two approaches. A superstructure based on separation tasks rather in actual columns is proposed. This approach is more flexibl...

A shortcut procedure as quick, easy-to use method for design and simulation of multicomponent batch distillation is used to predict the operating condition of recovering xylene from solvent in an existing batch distillation column in benzol refinery. The procedure can be used to investigate the effect of the operating parameters on the operation of column for three possible modes of batch d...

Batch distillation is one of the most important unit operations for the small-scale production of specialty and fine chemicals. The so called Middle Vessel Batch Distillation (MVBD) with total reflux offers many advantages compared to conventional batch distillation. It is favourable due to the simultaneous production of three products of high purity. In this work, we present a thorough analysi...

We used vortex contact devices that we developed and investigated to make a new design of an alcohol diabatic distillation column with heat exchange pipes (as the reflux condenser) passing through concentrating section trays. In column, ascending vapors partially condensed on surface vertically installed tubes, forming reflux. The was then mixed draining liquid flow in placed Heat removed from ...

−Dividing wall columns, capable of reducing the energy required for the separation of ternary mixtures, were explored for the energy-efficient integration of debutanization and deisobutanization. A new practical approach to the design and optimization of dividing wall columns was used to optimize dividing wall columns. A conventional dividing wall column and a multi-effect prefractionator arran...