نتایج جستجو برای: ray diffraction and ftir
تعداد نتایج: 16884555 فیلتر نتایج به سال:
Aluminum sulfate nano structures have been prepared by solution combustion synthesis using aluminum nitrate nonahydrate (Al(NO3)3.9H2O) and ammonium sulfate ((NH4)2SO4). The resultant aluminum sulfate nano structures were calcined at different temperatures to study thermal decomposition of aluminum sulfate. The crystallinity and phase of the as-synthesized and calcined samples were char...
The present study was carried out on the effect of acid leaching on the modification and structure alteration of montmorillonite. A nanostructured, activated material was prepared by selective leaching of pure smectite clay with different concentrations of sulfuric acid (1 10 N/L) at 85 ̊C for 120 min using a solid/liquid ratio of 1:20 and a reflux system. The Fourier transform infrared (FTIR), ...
In this research Calcium fluoride nanoparticles and its different amount of cerium ion dopant (5%and 10%) were prepared. The mentioned nanoparticle were studied by fourier transform infrared spectroscopy (FTIR) , X-ray diffraction (XRD), absorption and photoluminescence spectra (PL) and Scanning electron microscopy (SEM). The XRD patterns indicate a typical cubic fluorite structure and no other...
In the current research, effect of milling on the structure, particle size and morphology of montmorillonite was investigated. For this purpose, the montmorillonite was analyzed by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM). Then the montmorillonite was milled using high energy planetary ball mill at different milling times (1...
New forms of vanadium oxide Nanoporous were fabricated using a simple chemical synthesis method. Vanadium pentoxide (V2O5) Nanoporous were synthesized by sodium metavanadate as precursor and ethylene glycol as surfactant. The samples were characterized by high resolution transmission electron microscopy (HRTEM), field effect scanning electron microscopy (FESEM) and X-ray diffraction (XRD), Four...
lithium disilicate nano-powders were synthesized via a mild condition hydrothermal reaction at 180 ºc for 48 and 72 h with a non stoichiometric1:2 li:si molar ratio in naoh aqueous solution using li2co3 and sio2.h2o as raw materials. the synthesized materials were characterized by powder x-ray diffraction (pxrd) technique and fourier transform infrared (ftir) spectroscopy. the xrd data showed t...
Two new Cr(III) complexes based on 2-substituted 8-hydroxyquinoline ligands, namely [Cr(L₁)₃] (1), (HL₁=(E)-2-[2-(4-nitro-phenyl)-vinyl]-8-hydroxy-quinoline) and [Cr(L₂)₃] (2), (HL₂=(E)-2-[2-(4-chloro-phenyl)vinyl]-8-hydroxy-quinoline), were prepared by a facile hydrothermal method and characterized thoroughly by single crystal X-ray diffraction, powder X-ray diffraction, FTIR, TGA, ESI-MS, UV-...
In this research, Ce0.8Zr0.2-xMnxO2 nano particles (x = 0.0, 0.05, 0.10) were synthesized at 600 calcination temperature by co-precipitation method. The starting materials were cerium and zirconium nitrates, manganese chloride and ammonia as a precipitating agent. The crystalline structure of the synthesized samples was studied by X-ray diffraction (XRD) technique. TEM images of the prepared Ce...
Metal oxides play a very important role in many areas of chemistry, physics and materials science.The metal elements are able to form a large diversity of oxide compounds. In this investigation, wesynthesis SnO2 and C,N,S-tridoped SnO2 nanoparticles by precipitation method. The synthesizedSnO2 and C,N,S-tridoped SnO2 nanoparticles were characterized by instrumental analysis methods,such as X-ra...
we report on the synthesis, morphology, chemically and structurally of tio2-nio-sio2 nanostructure. the tio2-nio-sio2 nanostructure was synthesized by a method based on the sol-gel method, by the simultaneous gelation of all cations. the coatings were deposited on dried soda-lime glass slides by spin coating. composite powders and coating on glass have been characterized by xrd, sem, edax, and ...
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