Network Materials In article number 2207492, Niklas Wolff, Ion Tiginyanu, Lorenz Kienle, and co-workers report on the synthesis structural characterization of a hybrid wide-band-gap semiconductor nanocomposite network interconnected hollow microtubes composed β-Ga2O3/ZnGa2O4 phases using X-ray powder diffraction transmission electron microscopy. The aero-network morphology shows ZnGa2O4-dominat...

Natural products are normally obtained by organic solvent extraction and many subsequent chromatographic separations. Compounds of interest are often isolated with very low yield and limited purity. An aqueous two-phase extraction process combined with a simple ethanol treatment, for removing excess inorganic salt, has been developed for preparation of geniposide from gardenia. The system was c...

Ammonia-based selective catalytic reduction (SCR) has become the major control strategy for NOx emissions from light and heavy duty diesel engines. Before reducing NOx on the SCR active material, ammonia storage on the active sites of the catalyst is crucial. The in operando measurement of the dielectric properties of the catalyst material using microwave cavity perturbation is a promising indi...

In this research, we assessed the influence of an ultrafine 2CaO·SiO₂ powder on the hydration properties of a reactive powder concrete system. The ultrafine powder was manufactured through chemical combustion method. The morphology of ultrafine powder and the development of hydration products in the cement paste prepared with ultrafine powder were investigated by scanning electron microscopy (S...

OBJECTIVE The aim of this study was to evaluate the applicability of POVACOAT™, a hydrophilic PVA copolymer, as a solid dispersion (SD) carrier for hot-melt extrusion (HME). METHODS Bifendate (DDB), a water-insoluble drug, was chosen as the model drug. DDB was hot-melt extruded by a co-rotating twin screw extruder with POVACOAT™. The SD formability of POVACOAT™ was investigated by varying the...

The effect of proportion of maltodextrin and gum arabic as carrier material and the percentage of nutmeg oleoresin as flavor load on microencapsulation by spray drying was studied. The proportions of 0, 20, 40 and 60 percent gum arabic (w/w) in the carrier blend and 10, 20 and 30 percent nutmeg oleoresin (w/w) as flavor load were studied. Emulsions were microencapsulated in a vertical co-curren...

The identification of preferred binding domains within a host structure provides important insights into the function of materials. State-of-the-art reports mostly focus on crystallographic studies of empty and single component guest-loaded host structures to determine the location of guests. However, measurements of material properties (e.g., adsorption and breakthrough of substrates) are usua...

The metastable tetragonal Cu2Se phase as nanoflakes has been synthesized for the first time by treating CuCl2 taken in a mixture (1:1) of 1-octadecene and oleylamine with H2N-(CH2)3-SePh dissolved in 1-octadecene. Powder X-ray diffraction (PXRD), HRTEM, SEM-EDX and XPS have been used to authenticate the nanoflakes. The XPS of Cu2Se nanoflakes indicates oxidation states of Cu and Se as +1 and -2...

I summarize laboratory friction experiments on quartz powder sheared at room temperature and humidity. Slide-hold-slide experiments indicate that static friction and related parameters vary systematically with both hold time and loading velocity. The data indicate that healing is closely related to gouge porosity and that static friction and healing are not simple friction parameters, but rathe...

Series catalysts of Ru-SnOx/Al2O3 with varying SnOx loading of 0–3 wt% were prepared, and their catalytic activity and selectivity have been discussed and compared for the selective hydrogenation of m-dinitrobenzene (m-DNB) to m-nitroaniline (m-NAN). The Ru-SnOx/Al2O3 catalysts were characterized by X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy (XPS), transmission electron mi...