In this work, a fast and efficient microwave-assisted extraction (MAE) method was developed to extract main bioactive alkaloids from lotus plumue. To optimize MAE conditions, three main factors were selected using univariate approach experiments, and then central composite design (CCD). The optimal extraction conditions were as follows: methanol concentration of 65%, microwave power of 200 W, a...

An ionic liquids based simultaneous ultrasonic and microwave assisted extraction (ILs-UMAE) method has been proposed for the extraction of rutin (RU), quercetin (QU), from velvetleaf leaves. The influential parameters of the ILs-UMAE were optimized by the single factor and the central composite design (CCD) experiments. A 2.00 M 1-butyl-3-methylimidazolium bromide ([C4mim]Br) was used as the ex...

Given the growing tendency of consumers to choose products with natural ingredients, food industries have directed scientific research in this direction. In regard, algae are an attractive option for research, since they can synthesize a group secondary metabolites, called phenolic compounds, associated really promising properties and bioactivities. The objective work was classify major compare...

An ionic liquids (IL)-based microwave-assisted approach for extraction and determination of flavonoids from Bauhinia championii (Benth.) Benth. was proposed for the first time. Several ILs with different cations and anions and the microwave-assisted extraction (MAE) conditions, including sample particle size, extraction time and liquid-solid ratio, were investigated. Two M 1-butyl-3-methylimid...

the chemical speciation of heavy metals (arsenic, chromium, copper, lead, zinc and tin) in the sediments offormer tin mining catchment bestari jaya, peninsular malaysia was determined by using the latest version of the community bureau of reference, usually called the bcr 3-step sequential extraction procedure. furthermore, a fourth step was introduced for digestion and analysis of the residue....

Conventional extraction (CE) and microwave-assisted (MAE) were compared in terms of efficiency quality pectin two separate processes aimed to extract from Malus domestica ‘F?lticeni’ apple pomace. A similar yield a shorter time was observed for the procedure as CE, while galacturonic acid content degree esterification both methods. Apple extracted this plant source by methods had high content, ...

The LiMn1.5Ni0.5O4 spinel is an important lithium ion battery cathode material that has continued to receive major research attention because of its high operating voltage (∼4.8 V). This study interrogates the impact of microwave irradiation on the Mn(3+) concentration and electrochemistry of the LiMn1.5Ni0.5O4 spinel. It is shown that microwave is capable of tuning the Mn(3+) content of the sp...

Results of theoretical and experimental studies of a GW-class, large diameter microwave oscillator are presented. The device consists of a large cross-section (overmoded), slow-wave structure with a unique profile of wall radius specifically designed to support surface waves and to provide a strong beam-wave coupling at moderate voltage (500 kV), an internal adjustable microwave reflector, a co...