A new simple procedure for microwave-assisted organic synthesis under continuous flow processing has been developed for use in a monomodal microwave synthesizer with direct temperature control using the instrument's in-built IR sensor. This design makes optimum use of the standing wave cavity to improve the energy efficiency of microwave-assisted flow reactions.

This project deals with the problem at the core of chemical processes, that of creating a structure for the reaction-separation-recycle system. New methods have been developed for the synthesis of such structures capable of screening a wide range of options and taking account of all of the trade-offs simultaneously. For the first time these methods are capable of fully taking into account the i...

This paper presents a new approach for the simultaneous synthesis and optimization of heat integrated water networks. A new superstructure for heat exchanger network (HEN) synthesis is proposed. The procedure is based onmixed integer non-linearmathematical programming (MINLP). Four relevant examples are presented to illustrate various aspects of the proposed approach. © 2008 Elsevier Ltd. All r...

the nanoparticles of ti and tio2 have attracted extensive research interest because of their diverse applications in, for instance, catalysis, energy conversion, pigment and cosmetic manufacturing and biomedical engineering. through this project, a one-step bulk synthesis method of electromagnetic levitational gas condensation (elgc) was utilized for the synthesis of monodispersed and crystalli...

Aerosol synthesis methods for the production of nanostructured fullerene particles have been developed. The nanostructured, ultrafine fullerene particles were produced by vapor condensation and aerosol droplet drying and crystallization methods in tubular laminar flow reactors. The formation mechanisms were studied by measuring particle-size distributions is the gas phase. High-resolution scann...

the present article serves the purpose of pursuing geometrization of heat flow on volumetrically isothermal manifold by means of rf approach. in this article, we have analyzed the evolution of heat equation in a 3-dimensional smooth isothermal manifold bearing characteristics of riemannian manifold and fundamental properties of thermodynamic systems. by making use of the notions of various curva...

The partial oxidation of methane to synthesis gas was investigated in a novel type of perm selective membrane reactor using Perowskite hollow fibers. The operating behaviour of this membrane reactor integrating the process steps selective separation of oxygen from air, selective O2 transfer in the membrane and oxidation of methane with simultaneous steam reforming was investigated theoretically...

Light alkanes can be converted to more useful chemicals in noble metal coated monoliths at very short contact times. The short-contacttime reactor is described by detailed models for the flow field, chemistry, and their coupling. The partial oxidation of methane to synthesis gas in a rhodium coated monolith is studied numerically as an example. Keyword: reactor modelling, catalytic partial oxid...

While microwave enhancement of chemical syntheses has been demonstrated for a broad variety of chemical reactions, there is no accepted universal mechanism. Is the enhancement due to more efficient heating, to overheating, to nonuniform heating, or to nonthermal effects? Analyses are complicated due to the often significant spatial and temporal temperature variations in microwave reactor system...