Suspensions of Escherichia coli and Bacillus subtilis spores were exposed to conventional thermal and microwave energy at 2,450 MHz. The degrees of inactivation by the different energy sources were compared quantitatively. During the transient heating period by microwave energy, approximately a 6 log cycle reduction in viability was encountered for E. coli. This reduction was nearly identical t...

The control of nucleation in crystallization processes is a challenging task due to the often lacking knowledge on the process kinetics. Inflexible (predetermined) control strategies fail to grow the nucleated crystals to the desired quality because of the variability in the process conditions, disturbances, and the stochastic nature of crystal nucleation. Previously, the concept of microwave a...

Silver nanocubes were synthesized for the first time in large quantities on gold seed in the presence of a polyelectrolyte using microwave heating for 60-120 s. Our experiment indicates that the polyelectrolyte directs the growth of the particle in a specified crystallographic direction resulting in the faceted particle, i.e. a nanocube. The nanocubes are stable for at least 2 months in ambient...

The interaction of intense, femtosecond laser pulses with a dielectric medium is examined using a numerical simulation. The simulation uses the one-dimensional electromagnetic wave equation to model laser pulse propagation. In addition, it includes multiphoton ionization, electron attachment, Ohmic heating of free electrons, and temperature-dependent collisional ionization. Laser pulses conside...

The fabrication of hierarchical anatase microspheres with potential photocatalytic properties eventually comprises a consolidation step in which a high degree of crystalline order is typically achieved through conventional electric heating treatments. This however entails a substantial reduction in the specific surface area and porosity of the powders, with the consequent deterioration in their...

Three distinct sets of indole-based heterocycles were rapidly and selectively synthesized from the same set of Ugi-adducts under microwave heating in a reaction-condition-controlled manner. Notably, an unprecedented metal-free intramolecular sp(3)-hybridized C-H arylation using only cesium carbonate was discovered.

A microwave assisted extraction technique was developed to optimize the extraction of mucilage from the fruits of Abelmoschus esculentus plant. The plant has been extracted by conventional and microwave assisted methods for the isolation of mucilage. Microwave extraction at 160 W intensity and 40 min heating duration increase 11.55% in the yield of mucilage when compared to 1 h conventional hea...

Investigations of detection of high power microwaves in planar asymmetrically shaped microwave diodes on the basis of AlxGa1−xAs ternary semiconductors with various AlAs mole fraction are presented. The principle of operation of the microwave diodes is based on carrier heating phenomena in asymmetrically shaped homogeneous semiconductor structure due to different distribution of the electric fi...

The purpose of the study was to compare two methods for destruction of biological material for selenium (Se) analysis: wet digestion by conductive heating in programmed digestion block and digestion in microwave oven. In both methods samples were prepared in a closed system using nitric acid. Selenium was analysed by electrothermal atomic absorption spectrometry. The results have shown that bot...

The oxodiperoxo complex MoO(O2)(2)(tbbpy) (tbbpy = 4,4'-di-tert-butyl-2,2'- bipyridine) was isolated from the reaction of MoO2Cl(2)(tbbpy) in water under microwaveassisted heating at 120 masculineC for 4 h. The structure of the oxodiperoxo complex was determined by single crystal X-ray diffraction. The Mo(VI) centre is seven-coordinated with a geometry which strongly resembles a highly distorte...