in this work, zncao2 (zinc oxide-calcium oxide) nanocomposite were synthesized at different temperatures (500-700°c) by sol-gel method based on polymeric network of polyvinyl alcohol (pva). the synthesized samples were characterized by sem/edax, ft-ir and xrd techniques. it was found that synthesized nanocomposites have 1.62, 2.05 and 13.91%wt of cao, respectively. the obtained results show tha...

rapid and highly efficient synthesis of 2- or 2,5-substituted 1,3,4-oxadiazoles by the condensation of aryl carboxylic acid hydrazides and orthoesters can be achieved under microwave irradiation using an unmodified commercial over in unsealed vessels.

1, 8-dioxo-octahydroxanthene derivatives have efficiently been synthesized from dimedone and aromatic aldehydes using [fe(iii)(salen)cl] complex as an efficient and homogeneous catalyst in molten tetrabutyl ammonium bromide. this methodology offers several advantages, such as good yields, short reaction times, simple procedure, and mild conditions.

a simple and efficient procedure has been developed for the synthesis of 2,3-dihydroquinazolin-4(1h)-ones derivatives under solvent-free conditions. this method uses the condensation of isatoic anhydride, aldehydes, and amines in the presence of a catalytic amount sulfonated porous carbon (spc). one of the important advantages of the new method is that the spc could be recycled and reused.

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A new cyclic diarylheptanoid namely alnuheptanoid B (3), along with four known cyclic diarylheptanoids: myricanone (1), (+)-S-myricanol (2), myricanone 5-O--D-glucopyranoside (4), and (+)-S-myricanol 5-O--D-glucopyranoside (5) were isolated from the EtOAc fraction of Alnus japonica Steud (family: Betulaceae) stem bark. Their structures were established by different spectroscopic analyses, as ...