نتایج جستجو برای: crystallite size
تعداد نتایج: 556425 فیلتر نتایج به سال:
The preparation of Fe3O4 from ferrous salt by air in alkaline aqueous solution at various temperatures was proposed. The synthetic magnetites have different particle size distributions. We studied the properties of the magnetite prepared by chemical methods compared with magnetotactic bacterial nanoparticles. The results show that crystallite size, morphology, and particle size distribution of ...
Ion plating is essentially vapor deposition onto a substrate which is the cathode of a glow discharge. The most important characteristic of the technique is that the growing film is subjected to a flux of high energy particles (neutrals and ions). In this study we report information about the effect of ion plating parameters on grain diameter and crystallite size distribution. At a constant pot...
The synthesis of nano- structured cobalt through a controlled chemical process followed by heat treating at various temperatures is studied. The product is characterized by ICP, XRD, FESEM , and TEM, indicating that the as- synthesized particles have an amorphous structure with 1.76 for Co/B ratio, an average size of 50 nm. The transformation of intermediate phases into single phase nano- cryst...
Nanostructure Forsterite powder was prepared by Sol-gel method and its microstructure was studied at a number of annealing temperatures using Rietveld structure and microstructure refinements. It was found that Sol-gel method used in this experiment does not produce pure Mg2SiO4 nanopowder. Instead the product is a mixture of Mg2SiO4 and MgO phases with approximate weight fractions of 75% and 2...
Arc-melting with ball milling was used for preparing Fe2CoGa1+x and Co2FeGa1+x (x=0,0.2) Heusler samples. Effect of extra nonmagnetic Ga atoms on lattice ordering and magnetic properties of Fe2CoGa and Co2FeGa Heusler compounds was studied. Rietveld refinement showed that lattice parameter of the samples increases in the presence of extra Ga atoms. Results showed that Co2FeGa1.2 has a partial ...
Iron oxide nanoparticles have received sustained interest for biomedical applications as synthetic approaches are continually developed for control of nanoparticle proper‐ ties. However, many approaches focus solely on the material, rather than the complete optimization of synthe‐ sis and functionalization together to enhance translation into biological systems. Presented herein is a modified s...
In this work, cobalt ferrite nanocrystallites were synthesized by air annealing of milled Co-Fe compound. Effect of annealing temperature on phase formation of cobalt ferrite and structural and magnetic properties of the product was studied. Analysis of annealed sample in 450 oC showed that around 46 weight percent of the specimen was changed to Co2FeO4. This value increased to 95 and 90% for 8...
Zn0.9Co0.1O ceramic pigments were synthesized using simple high energy milling method. Zinc and cobalt oxides were used as starting materials. Products were investigated using simultaneous thermal analysis and fourier transformation infrared. Pigments were characterized using X-ray diffraction, diffuse reflectance and Scanning Electron Microscopy. The results showed the effect of calcination te...
In this research, Cu0.5Zn0.5Fe2O4 nanoparticles were prepared by citrateprecursormethod and under air-ambient annealing at 200, 400, 600°C. The structural features of samples were investigated by X-ray powder diffraction and FT-IR spectroscopy. The structural characterization of compounds, using X’Pert package and Fullprof program, is evidence for formation of a cubic structure (Fd-3m space gro...
mechanical alloying of binary and ternary elemental powder mixtures with the nominal compositions of mg2ni and mg(2-x)mnxni (x= 0, 0.05, 0.10 and 0.15 at. %) were carried out in a planetary ball mill for various milling times of 5, 10, 15, 20, 30 and 60 h. x-ray diffraction and field emission scanning and transmission electron microscopy were used for the characterization of the milled products...
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