A microwave-assisted digestion method for the determination of cadmium (Cd) and lead (Pb) by inductively coupled plasma mass spectrometry (ICP-MS) was optimised on certified reference material (CRM) (bovine liver, BCR-185R) and wolf liver samples. Different factors influencing digestion efficiency (temperature, time, composition of the digestion mixture, sample mass) were tested. Validation inc...

The effects of various additives on the physical properties of an amorphous sugar matrix were compared. Amorphous, sugar-additive mixtures were prepared by freeze-drying and then rehumidified at given RHs. Sucrose and eighteen types of substances were used as the sugar and the additive, respectively, and water sorption, glass-to-rubber transition, and protein stabilization during freeze-drying ...

The fine structure of the regular arrays of subunits seen on both plasmalemma fracture faces in resting and starved Saccharomyces cerevisiae (baker's yeast) has been compared using different freeze-fracture replication methods. Freeze-cleaving was carried out at 173 degrees, 133 degrees, and 108 degrees K under a vacuum of 2 X 10(-7) torr (2.6 X 10(- 7)mbar) or under liquid nitrogen at atmosphe...

A bstract The vanishing of the Higgs quartic coupling at a high energy scale may be explained by Intermediate Scale Supersymmetry, where supersymmetry breaks (10 9 -10 12 ) GeV. possible range breaking scales can narrowed down precise measurements top quark mass and strong constant. On other hand, nuclear recoil experiments probe Higgsino or sneutrino dark matter up to 10 We derive correlation ...

The relativistic hydrodynamic approach is used to describe production of strangeness and/or heavy quarks in ultrarelativistic heavy ion reactions. Production processes are important ingredients of dissipative effects in the hadronic liquid. Beyond viscosity also chemoand thermo-diffusion processes are considered. This also allows to specify chemical and thermal freeze-out conditions. Submitted ...

INTRODUCTION From a series of radiolabelled cholecystokinin (CCK) and gastrin analogues, (111)In-CP04 ((111)In-DOTA-(DGlu)6-Ala-Tyr-Gly-Trp-Met-Asp-Phe-NH2) was selected for further translation as a diagnostic radiopharmaceutical towards a first-in-man study in patients with medullary thyroid carcinoma (MTC). A freeze-dried kit formulation for multicentre application has been developed. We here...

A comparison was made of the relative efficiencies of three enrichment media, RapidChek Escherichia coli O157:H7 enrichment broth (REB), R&F broth (RFB), and modified E. coli broth containing novobiocin (mEC+n), and four selective plating media for detection of cold- and freeze-stressed E. coli O157:H7 in raw ground beef. Ground beef (25 g) was inoculated with E. coli O157:H7 at < or =0.5 and <...

Abstract Carotenoids were recovered from carrot processing waste using sunflower oil. Simplex centroid mixture design was applied for the optimization of wall material formulations (whey protein/maltodextrin/inulin) encapsulation extract by freeze drying (FD) and spray (SD). The optimal materials pure whey protein , 71 g/100 g - 29 g/100 g inulin mixture, respectively, showing total carotenoids...

With the objective of developing new advanced composite materials that can be used as anodes for lithium ion batteries (LIBs), herein we describe the synthesis of a novel three dimensional (3D) macroporous foams formed by reduced graphene oxide (rGO) and submicron tin-based particles. The aerogels were obtained by freeze/freeze-drying a suspension of graphene oxide (GO) in the presence of a tin...

In experiments in which liver and testis freeze-stops were performed on pentobarbital-anaesthetized rats, ethanol (1.5 g/kg body wt.) reduced plasma testosterone concentration from 13.1 to 3.2 nmol/litre. 4-Methylpyrazole abolished the ethanol-induced hepatic and testicular increase in the lactate/pyruvate ratio, and the testicular acetaldehyde level, but did not diminish the reduction in plasm...