the most used quechers and gas chromatography methods were performed, to evaluate the presence of organochlorines, organophosphate, polychlorinated biphenyl and chlorobenzenes in water and in fish. according to the standard iso iec 17025, a recovery rate obtained ranged from 70 to 120% assessing the reliability of analysis results. the exceed rate in fish of malathion is 22.2, and 5.2 ppm in sa...