The chemical composition, anatomical characteristics, lignin distribution, and cell wall structure of oil palm frond (OPF), coconut (COIR), pineapple leaf (PALF), and banana stem (BS) fibers were analyzed. The chemical composition of fiber was analyzed according to TAPPI Methods. Light microscopy (LM) and transmission electron microscopy (TEM) were used to observe and determine the cell wall st...

Gold nanoparticles (NPs) were assembled and cross-linked into spherical aggregates by colloidal emulsion evaporation and ligand exchanging. The optical absorption, conventional transmission electron microscopy (TEM) and bright field (BF) TEM tomography confirm that the cross-linking of the pre-condensed aggregates generates high stability and compactness.

Here we present time-resolved in situ transmission electron microscopy (TEM) observations and real-time manipulation of nematic ordered cellulose and ultradrawn polyethylene films. Drawn films of these two polymers exhibited a unique response to the low-dose electron beam. Electron beam damage was minimal based on retention of an organized electron diffraction pattern. Increased electron dosage...

Anodic self-organized TiO2 nanotube layers (with different aspect ratios) were electrochemically infilled with CuInSe2 nanocrystals with the aim to prepare heterostructures with a photoelectrochemical response in the visible light. The resulting heterostructure assembly was confirmed by field-emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), and X-ray diffra...

colloidal nanosilica is currently being produced by various methods which are mainly high energy intensive and/or not environmentally friendly. it is therefore essential to develop new energy-efficient and environmentally friendly technologies. this paper introduces a new ultrasound assisted route based on alkali leaching of silica fume for synthesis of colloidal silica nanoparticles. the ef...

In this study, mononuclear octahedral cobalt(III) Schiff base complex [CoL3], L = (5-bromo-2-hydroxybenzyl-2-furylmethyl)imine, was synthesized from the reaction of Co(NO3)2•6H2O and the Schiff base ligand L in methanol as solvent. It used as a new precursor to prepare spinel type cobalt oxide nanoparticles by a facile solid-state thermal decomposition. Controlling the temperature and time, Co3...

We report the preparation and characterization of spinel-structured FeCo2O4 nanoparticles for the efficient and selective oxidation of sulfides. The as-prepared FeCo2O4 nanoparticles were characterized by powder X-ray diffraction (PXRD), energy-dispersive X-ray analysis (EDX), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). According to TEM images, the size of the...

zinc oxide nanotubes were prepared by a hydrothermal method using zinc nitrate as a precursor. The synthesized nanotubes were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR) and their optical properties were characterized using UV -visible spectroscopy. The XRD analysis confirme...

There is great motivation in the electron microscopy field to speed up and streamline sample processing, especially for transmission electron microscopy (TEM) which can take days to weeks to complete on the bench. The sample processing microwave has been developed to allow faster protocols, and tissue processors have automated the procedure, but as yet there is no established combination of spe...

in this work, the template, monomer and cross-linker with the ratio of 1:8:40 were used to synthesize molecularly imprinted polymers (mips) for extraction of the bioactive chemical compounds from some traditional herbs as a sorbent material. quercetin, methacrylic acid (maa), trimethylolpropanetrimethacrylate (trim) and tetrahydrofuran (thf) were used as a template, functional monomer, cross-li...