نتایج جستجو برای: particle preparation
تعداد نتایج: 345472 فیلتر نتایج به سال:
Dispersed particle gel (DPG) has been first successfully prepared using cross-linked gel systems through a simple high speed shearing method with the aid of a colloid mill at room temperature. The gel microstructure and particle size were investigated by scanning electron microscope (SEM), transmission electron microscope (TEM), and dynamic light scattering (DLS) measurements. The results clea...
In one of the current histochemical methods for dehydrogenases and diaphorases the final product is a metal-formazan dye derived from reduction of an N-thiazolyl-substituted tetrazolium. Sites of enzymic activity consistently appear as intramitochondrial dots 0.2 to 0.3 micro in diameter. When applied to active particles from disrupted mitochondria (Keilin-Hartree preparation, electron transpor...
By contrast to traditional free radical emulsion polymerization, catalytic polymerization allows for polymer microstructure control. In terms of monomers polymerizable, both techniques are largely complementary. Since the beginning of this decade, an increasing number of reports on polyolefin, polybutadiene, polyalkenamer, polynorbornene, polyketone and polyacetylene dispersions prepared by cat...
We investigated the relations between the yield stress of polar-molecule dominated electrorheological (PM-ER) fluids and the shape of ellipsoidal particles of the fluids. It is found that, when the short axis of an ellipsoidal particle is along an external electric field while the volume of the particle keeps constant, the shorter of the short axis is, the stronger the attraction between the tw...
The formation of pure single crystalline silicon nanoparticles by microwave induced decomposition of silane in a low pressure flow reactor is reported. The morphology and crystal structure of the particles are characterized in situ by particle mass spectrometry (PMS) and ex situ by means of X-ray diffraction, high resolution transmission electron microscopy, electron energy loss spectroscopy, a...
We provide an explicit analytical calculation that shows the asymptotic approach of the one dimensional Caldeira-Leggett model to thermal equilibrium in the high temperature and weak coupling limit. We investigate a free particle and a harmonic oscillator system, using both the Lindblad and the nonLindblad type master equations for each case, and show that thermal equilibrium is reached exactly...
We prepare packings of frictional tetrahedra with volume fractions ϕ ranging from 0.469 to 0.622 using three different experimental protocols under isobaric conditions. Analysis via x-ray microtomography reveals that the contact number Z grows with ϕ, but does depend on the preparation protocol. While there exist four different types of contacts in tetrahedra packings, our analysis shows that t...
We report a simple method for the preparation of magnetically-functionalized lens-like and donut-shaped polymeric microparticles, based on spreading a magnetite-doped paraffin-polymer solution at the air/water interface in the presence of an external magnetic field. We examine the parameters that affect the particle morphology and interfacial aggregation behaviour.
Supercritical fluid technologies (SCFT) represent a recent approach for obtaining pharmaceutical materials in pure physical form and the application of supercritical fluids is a superior alternative to conventional precipitation and extraction processes. Supercritical fluid technology (SCFT) offers exciting opportunities to produce and modify pharmaceutical substances and has the potential to r...
We report the preparation and properties of an electron-dense antibody conjugate, made by the covalent bonding of an iron-dextran (Imposil) particle to an antibody molecule. Transmission electron microscopic experiments with the Imposil-antibody conjugates demonstrate their suitability as specific immunostains at high resolution, particularly for simultaneous double staining experiments in conj...
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