By coupling techniques of simultaneous secondary (SE) and transmitted electron (TE) imaging at high resolution in a modern scanning transmission electron microscope (STEM), with the ability to heat specimens using a highly stable MEMS-based heating platform, we obtained synergistic information to clarify the behavior of catalysts during in situ thermal treatments. Au/iron oxide catalyst 'leache...

A new facile coating strategy based on the hydrophobicity of methyl groups was developed to prevent nano-sized magnetite particles from strong acid corrosion. In this method, three steps of hydrolysis led to three layers of protection shell coating Fe3O4 nanoparticles. Filled with hydrophobic methyl groups, the middle layer mainly prevented the magnetic core from strong acid corrosion. These ma...

Magnetotactic bacteria are characterized by the magnetosome, a membrane-bound, nano-sized organelle containing a magnetic crystal. This organelle is believed to help the bacteria to navigate along the geomagnetic field lines and find a preferred habitat for survival. The magnetosome is a biomineral structure highly controlled by the bacteria, composed of either magnetite (Fe3O4) or greigite (Fe...

Abnormal accumulation of brain metals is a key feature of Alzheimer's disease (AD). Formation of amyloid-β plaque cores (APC) is related to interactions with biometals, especially Fe, Cu and Zn, but their particular structural associations and roles remain unclear. Using an integrative set of advanced transmission electron microscopy (TEM) techniques, including spherical aberration-corrected sc...

We report a facile method to produce a magnetically separable graphene oxide–magnetite nanocomposite (GO–Fe3O4) and its adsorption performance in methylene blue (MB) removal from aqueous solution. The GO–Fe3O4 nanocomposite was synthesized by a solution-phase self-assembly method including the incorporation of monodisperse Fe3O4 nanoparticles (NPs) and GO in a dimethylformamide/chloroform mixtu...

BACKGROUND Because of their unique magnetic properties, Fe3O4 nanoparticles (Fe3O4-NPs) have extensive applications in various biomedical aspects. Investigation of the possible adverse aspects of these particles has lagged far behind their fast growing application. OBJECTIVES The current study aimed to evaluate the toxicity of Fe3O4-NPs in the liver of mice. MATERIALS AND METHODS In the pre...

We describe here a simple synthetic strategy for the fabrication of carbon-coated Fe3O4 (Fe3O4@C) particles using a single-component precursor, iron (III) diethylenetriaminepentaacetic acid complex. Physicochemical analyses revealed that the core of the synthesized particles consists of ferromagnetic Fe3O4 material ranging several hundred nanometers, embedded in nitrogen-doped graphitic carbon ...

Introduction : Nowadays, using drug delivery is an essential method to improve cancer therapy through decreasing drug toxicity and increasing efficiency of treatment. Silibinin (C25H22O10), a polyphenolic flavonoid which is isolated from the milk thistle plant, has various applications in cancer therapy but it has hydrophobic structure with low water solubility and bioavailability. To increase ...

A magnetic Fe3O4/GO composite with potential for rapid solid-liquid separation through a magnetic field was synthesized using GO (graphene oxide) and Fe3O4 (ferriferous oxide). Characterization of Fe3O4/GO used scanning electron microscope (SEM), X-ray diffractometer (XRD), Fourier transform infrared spectrometer (FT-IR), and Vibrating Sample Magnetometer (VSM). A number of factors such as pH a...

Ảnh hưởng của nhiệt độ ủ lên cấu trúc, hình thái và tính chất từ các mẫu bột tổ hợp nano Fe/Fe3O4 đã được khảo sát. Các chế tạo bằng cách kết giữa nghiền bi năng lượng cao tại 623, 723 823 K. Cấu đặc trưng bởi nhiễu xạ tia X, hiển vi điện tử quét. phép đo này chỉ ra sự tiến triển pha tinh thể khi tăng. Đồng thời thay đổi bất thường khác nhau: dạng hạt (623 K), lá (723 K) thanh (823 K). phòng ch...