A solid-phase extraction (SPE) method for sample clean-up and preconcentration followed by reversed-phase high-performance liquid chromatography (RP-HPLC) with uv detection is reported for determination of polycyclic aromatic hydrocarbons (PAHs) in the caspian seawater. A good resolution was obtained using acetonitrile:water (40:60) as mobile-phase for separation of these compounds. The eff...

Carbon nanotubes (CNTs) possess unique mechanical, physical, electrical and absorbability properties coupled with their nanometer dimensional scale that renders them extremely valuable for applications in many fields including nanotechnology and chromatographic separation. The aim of this review is to provide an updated overview about the applications of CNTs in chiral and achiral separations o...

background: 66ga (t1/2=9.49 h, β+: 4.153 mev, γ: 511, 834, 1039, 2752 kev) has a wide range of applications in different fields of medical sciences. production of 66ga became one of our main interests, according to its increasing applications in nuclear medicine, particularly in pet imaging. materials and methods: 66 zn (p,n)66ga reaction was determined as the best choice for the production of ...

a solid-phase extraction (spe) method for sample clean-up and preconcentration followed by reversed-phase high-performance liquid chromatography (rp-hplc) with uv detection is reported for determination of polycyclic aromatic hydrocarbons (pahs) in the caspian seawater. a good resolution was obtained using acetonitrile:water (40:60) as mobile-phase for separation of these compounds. the effect ...

Liquid chromatography is a very important separation method used in practically all chemistry fields. For many decades, it has played a key role in academic and industrial laboratories where it is used to analyze or purify components from complex mixtures. For example, it is used to separate proteins/drugs from impurities and to analyze drugs and endogenous components in biological materials. M...

A review is presented of sample preparation and separation techniques for the determination of inorganic ions by ion chromatography (IC) and capillary electrophoresis (CE). Emphasis has been placed on those sample treatment methods which are specific to inorganic analysis, and the developments in separation methods which are discussed are those which enhance the capabilities of IC and CE to han...

Size exclusion chromatography (SEC) has been widely applied in protein separation based on their molecular sizes. Here we present a peptide mixture from 1kD to 6 kD separation on size exclusion chromatography column Zenix TM -80. The effect of different mobile phases on the peptides’ separation performances was also explored. In the separation of insulin, glucagon, angiotensin I and bradykinin,...

Reversed-phase chromatography is a method that is often used for glycan separation. For this, glycans are often derivatized with a hydrophobic tag to achieve retention on hydrophobic stationary phases. The separation and elution order of glycans in reversed-phase chromatography is highly dependent on the hydrophobicity of the tag and the contribution of the glycan itself to the retention. The c...

As a new type of environmental pollutant, microplastics (MPs) exists in the soil environment for long time and pollutes ecological surface system. Separation detection is basis controlling pollution environment. The research progress separation technology was introduced, existing problems methods were put forward. results show that screening-filtration method density are simple, operable effect...

499: 177. Lindner H, Sarg B and Helliger W (1997) Application of hydrophilic-interaction liquid chromatography to the separation of phosphorylated H1 histones. Journal of Chromatography 728: 55. Mant CT and Hodges RS (eds) (1991) High-performance Liquid Chromatography of Peptides and Proteins: Separation, Analysis, and Conformation. Boca Raton: CRC Press. Mant CT and Hodges RS (1996) Analysis o...