نتایج جستجو برای: dispersive liquid liquid microextraction based on solidification of floating organic drop

تعداد نتایج: 22145865  

Journal: :iranian journal of public health 0
hamid shirkhanloo 1. iranian petroleum industry health research institute (ipihri), occupational and environmental health research center (oehrc) , tehran, iran. farideh golbabaei 2. dept. of occupational health engineering, school of public health, tehran university of medical sciences , tehran, iran. hamid hassani 2. dept. of occupational health engineering, school of public health, tehran university of medical sciences , tehran, iran. farrokh eftekhar 1. iranian petroleum industry health research institute (ipihri), occupational and environmental health research center (oehrc) , tehran, iran. mohammad javad kian 1. iranian petroleum industry health research institute (ipihri), occupational and environmental health research center (oehrc) , tehran, iran.

exposure to mercury (hg) as a heavy metal can cause health effects. the objective of this study was to assess occupational exposure to hg in a chlor-alkali petrochemical industry in iran by determining of hg concentrations in air, blood and urine samples.the study was performed on 50 exposed subjects and 50 unexposed controls. air samples were collected in the breathing zone of exposed subjects...

Journal: :Chemija 2022

In this study, eight hydrophobic supramolecular (SUPRA) solvents composed of tetrabutylammonium chloride and tetradecyltrimethylammonium bromide as amphiphiles four perfluorinated compounds (hexafluoroisopropanol, trifluoroacetic acid, pentafluoropropionic acid heptafluorobutyric acid) coacervation-inducing agents were developed. The SUPRA phase volumes determined a function individual concentr...

Journal: :Talanta 1969
T Fujinaga T Kuwamoto E Nakayama

A low-melting solid is used as organic solvent for liquid-liquid extraction at elevated temperatures followed by solidification and decantation of the aqueous phase.

Razieh Zakerian Soleiman Bahar,

In this study, we combined Ionic Liquid-based Dispersive Liquid Liquid Micro Extraction (IL-DLLME) with FAAS for determining the palladium in different real samples at the trace level. 1-hexyl-3-methylimidazolium hexafluorophosphate [Hmim][PF6] ionic liquid and 1-(2-pyridylazo) 2-naphthol (PAN), were chosen as the extraction solvent and the chelating agent, respectively. The hydr...

Journal: :international journal of environmental research 2014
h. sereshti n. eskandarpour s. samadi gh. aliakbarzadeh

the task specific ionic liquid (tsil), tricaprylmethylammonium thiosalicylate ([a336][ts]),was synthesized, characterized and subsequently used as extraction solvent in dispersive liquid-liquidmicroextraction (dllme) technique. the tsil-dllme method followed by inductively coupled plasmaatomicemission spectrometry (icp-aes) was applied to determination of trace mercury (hg) and cadmium(cd) in a...

Journal: :Acta poloniae pharmaceutica 2017
Anna Petruczynik Monika Waksmundzka-Hajnos

The review of the RP HPLC analysis of basic psychotropic drugs is presented. It contains sample preparation methods with centrifugation, protein precipitation, liquid-liquid extraction (LLE), dispersive liquid-liquid microextraction (DLLME), solid-phase extraction (SPE), solid-phase microextraction (SPME), microwave-assisted extraction (MAE) and RP-HPLC analysis. Chromatographic behavior of bas...

Journal: :Cumhuriyet Science Journal 2022

In this research paper, a simple and economic ionic liquid-based liquid-liquid microextraction (IL-DLLME) procedure was developed to ensure efficient rapid separation preconcentration of erythrosine from cosmetic food samples. Important parameters such as IL volume, temperature, acetone ultrasonic time pH that may affect the IL-DLLME have been optimized by central composite design (CCD) based o...

پایان نامه :وزارت علوم، تحقیقات و فناوری - دانشگاه یزد 1388

روش میکرواستخراج قطره آلـی منجمد شنـاور شده (solidified floating organic drop microextraction) همراه با اسپکتروفتومتری بـرای جـداسازی/ تغلیظ و انـدازه گـیری مقادیر ناچیز وانـادیـم در نمونه هـای آب طراحی شده است. از 8- هیدروکسی کینولین ( اکسین ) به عنوان عامل کـی لیت دهنده استفاده شده است. در این مطالـعه پـارامترهـای موثر بر سیستم استـخـراج مانند ph، ماهیت حلال آلی، غلظت اکسین، حجم فاز آلی، زمان...

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