In this research, YBa2Cu3O7-d (0 < d < 1) nanocrystalite superconductor was prepared by mechanochemical alloying method. We synthesized YBa2Cu3O7-d via mixing the BaCO3, Y2O3, CuO powders and milling in SPEX 8000 for 5h with weight ratio of ball to powder 10:1 and steel balls of 11mm diameter, followed by heating for 4h at 850 ˚C. The superconductor phase formation process was completed with si...