Stoichiometric compositions of NiO were prepared by the standard chemical co-precipitation method to inspect effect calcination temperature on structures, morphology, and physical properties. The samples calcined at three different temperatures viz. 350 °C, 550 650 °C for 5 h. X-ray diffraction analysis confirmed cubic (Fm-3m) structure samples. average crystalline size increases from 41 nm abo...

In this work, the effect of carbon dioxide partial pressure on the calcination kinetics of high purity zinc carbonate hydroxide has been studied. Non-isothermal analysis has been performed on samples at different CO2 partial pressures by TGA and DTA. It has been found that the calcination behaviour of this material corresponds to the shrinking core model and the reaction mechanism is phase boun...

In this work, two types of solvents ethanol or water were used in preparation of the LaFeO3 catalysts by citrate sol gel method. The obtained samples were subjected to various calcination temperatures in order to study the catalytic activity and stability for methanol electro-oxidation by XRD, cyclic voltammetry and chronoamperometry. The crystallinity of the LaFeO3 ph...

nanocrystalline zno particles were prepared by a novel sonochemical route from zinc acetate and sodium hydroxide without any requirement of calcination steps at high temperature and without surfactants. variations in several parameters and their effects on the structural (crystal size and morphology) properties of nanoparticles were investigated. characterizations were carried out by x-ray diff...

in this study, copper chromite (cucr2o4) nanoparticles was prepared by inverse co-precipitation method. in this method, cupric nitrate trihydrate, (cu (no3)2.3h2o) and chromium nitrate nonahydrate, (cr (no3) 3.9h2o) with a mole ratio of 1:2 were used. characterization of cucr2o4 nanoparticles was performed by fourier transform infrared spectroscopy (ft-ir), raman spectroscopy, x-ray diffraction...