Surface orientation plays an important role in the oxidation behavior of single crystals where studies have found the relative oxidation rates for surfaces with different orientations. However, most materials are polycrystalline and contain myriad orientations that contribute to the overall oxidation process. Here we determine the effects of orientation on the early stages of oxidation behavior...

Calcium Tschermak’s pyroxene (CaTs), CaAlAlSiO6, is well known as an important component in pyroxene. It is a member of the Ca clinopyroxene group in which Al dominates in the M1 site. Pyroxenes with more than 80 mol% CaTs were observed previously in Ca-,Al-rich refractory inclusions (CAI) from five carbonaceous chondrites. This study re-investigated the near end-member CaTs in the Allende and ...

The response of materials after microscale laser shock peening (mLSP) was experimentally characterized and compared with the theoretical prediction from FEM analysis in microlength level. Since mLSP is predominantly a mechanical process instead of a thermal process, the characterization focuses on mechanical properties and associated microstructures. An X-ray microdiffraction technique was appl...

The {101} transformation twinning bands in Mn–Cu alloys are considered to be the dominant microstructural feature contributing to the high damping capacity of the alloys. Because the face-centered-tetragonal (fct) phase of Mn–Cu alloys has an axis ratio ðc=aÞ of nearly 1, an angular resolution for Kikuchi diffraction bands of better than 0.5 is necessary to identify the twin boundaries by the e...

An Al–3% Mg–0.2% Sc alloy was solution treated and processed through 10 turns of highpressure torsion (HPT) at 450 K. Afterwards, the HPT-processed alloy was annealed for 1 h at temperatures ranging from 423 to 773 K and its mechanical properties and microstructural evolution were examined using microhardness measurements and electron backscattered diffraction (EBSD) analysis. The results demon...

We report the crystallization of electrodeposited germanium (Ge) thin films on n-silicon (Si) (100) by rapid melting process. The electrodeposition was carried out in germanium (IV) chloride: propylene glycol (GeCl₄:C₃H₈O₂) electrolyte with constant current of 50 mA for 30 min. The measured Raman spectra and electron backscattering diffraction (EBSD) images show that the as-deposited Ge thin fi...

An Al-3%Mg-0.2%Sc alloy was processed by ECAP and HPT at different temperatures. Afterwards, samples subjected to 10 turns of HPT at 300 and 450 K, 8 passes of ECAP at 300 K and 10 passes of ECAP at 600 K were annealed for 1 hour at 523 K and their mechanical properties and microstructure were examined using microhardness measurements and EBSD analysis. In addition, tensile specimens with simil...

The microstructure stability during d sub-solvus annealing in Inconel 718 was investigated, focusing on the conditions that may lead to the development of very large grains (about 100 lm) in a recrystallized fine grained matrix (4 to 5 lm) despite the presence of second-phase particles. Microstructure evolution was analyzed by EBSD (grain size, intragranular misorientation) and SEM (d phase par...