Among the possible variants of X-Ray Fluorescence (XRF), applications exploiting scanning Macro-XRF (MA-XRF) are lately widespread as they allow visualization element distribution maintaining a non-destructive approach. The surface is scanned with focused or collimated X-ray beam millimeters less: analyzing emitted fluorescence radiation, also elements present below contribute to elemental imag...

Following QA/QC procedures, portable XRF (p-XRF) field tests were performed on borehole samples from nickel laterite deposits and the results compared with lab-XRF results. To verify reliability accuracy of obtained by p-XRF in field, certified reference materials prepared as glass beads analyzed together samples. The showed that overall contents each element generally lower wet than pulp sampl...

this study is aimed to identify sources of particulate matter with mean aerodynamic diameterbelow 10 μm (pm10) present in the atmosphere of the metropolitan area of mexico city (mamc), usingsamples obtained from january 1st to june 30th, 2009, analyzed with x-ray spectrometric techniques.minivol samplers were used to collect samples on polycarbonate filters in three sites (north, center, andsou...

Synchrotron-based micro-X-ray fluorescence (micro-XRF) and micro-X-ray absorption spectroscopy (micro-XAS) were used in the present study to obtain spatially resolved micro-scale information on elemental composition, trace element distribution, chemical speciation and oxidation state and/or mineral phase distribution within historical iron artefacts dating from the Iron Age to early Medieval Ti...

The legacy of planetary X-ray Diffraction (XRD) and X-ray Fluorescence (XRF) began in 1960 when W. Parish proposed an XRD instrument for deployment on the moon. The instrument was built and flight qualified, but the Lunar XRD program was cancelled shortly before the first human landing in 1969. XRF chemical data have been collected in situ by surface landers on Mars (Viking 1 & 2, Pathfinder) a...

Preparing dry specimens from liquid samples for XRF analysis avoids introducing caustic or hazardous liquids into the instrument. Several modifications were made to a dried residue specimen preparation method for quantifying gallium in plutonium metal in order to improve the method accuracy and precision. Ion exchange chromatography was utilized to remove the plutonium prior to casting the drie...

the most used quechers and gas chromatography methods were performed, to evaluate the presence of organochlorines, organophosphate, polychlorinated biphenyl and chlorobenzenes in water and in fish. according to the standard iso iec 17025, a recovery rate obtained ranged from 70 to 120% assessing the reliability of analysis results. the exceed rate in fish of malathion is 22.2, and 5.2 ppm in sa...