The aim of the current work is the synthesis and characterization of metallic Zr nanoparticles. The preparation is carried out by using the RAPET method (Reaction under Autogenic Pressure at Elevated Temperatures) developed in our lab. The RAPET reaction of commercial ZrO(2) with Mg powder was carried out in a closed stainless steel cell, at 750 °C. On completion of the reaction, the additional...

The performances of cementitious materials as well as the efficiency of construction are adversely affected at high temperatures. Previous studies have already demonstrated that ultra-fine (alccofine) material accelerates the hydration of cement particles and subsequently improves the mechanical and durability properties of the concrete at normal temperature. Moreover, at higher temperatures th...

Bioapatite, the main constituent of mineralized tissue in mammalian bones, is a calcium-phosphate-based mineral that is similar in structure and composition to hydroxyapatite. In this work, the crystallographic structure of bioapatite in human fetuses was investigated by synchrotron radiation x-ray diffraction (XRD) and microdiffraction ( micro -XRD) techniques. Rietveld refinement analyses of ...

This article introduced the work of ethylcellulose based polymeric microsphere loaded with nifedipine for reduction in frequency of administration with low solubility in aqueous medium and high rate of absorption in the stomach. The non-aqueous polymeric suspension was put dropwise into an aqueous medium containing polyvinyl alcohol as a surfactant for the synthesis of microsphere by solvent ev...

The thermoluminescence (TL) after excitation by UV or X-rays radiation of alumina-zirconia powders is investigated. The composites present five of the characteristic peaks of zirconia at −170, −145, −90, 0 and 95 °C. After a thermal treatment of mixed oxides, a new peak is observed at −35 °C in TL. This peak reveals the presence of stabilized tetragonal zirconia in the material. Moreover by com...

Inspired green synthesis of metallic nanoparticles is evolving as an important branch of nanotechnology. Traditionally these are manufactured by wet chemical methods which require toxic and flammable chemicals. We report for the first time an economic and eco-friendly green synthesis of silver nanoparticles using Strychnos potatorum aqueous leaf extract from 3 mM silver nitrate solution. Nanopa...

Titanium dioxide nanopowders doped with different amounts of Fe ions were prepared by coprecipitation method. Obtained materials were characterized by structural (XRD), morphological (TEM and SEM), optical (UV/vis reflection and photoluminescence, and Raman), and analytical techniques (XPS and ICP-OES). XRD analysis revealed rutile crystalline phase for doped and undoped titanium dioxide obtain...

We carried out a residual stress distribution analysis in a APS TBC throughout the depth of the coatings. The samples were heat treated at 1150 °C for 190 h and the data analysis used image based modelling based on the real 3D images measured by Computed Tomography (CT). The stress distribution in several 2D slices from the 3D model is included in this paper as well as the stress distribution a...

The purpose of the study was to investigate the mineralogical and Heavy Metals (HMs) present in the granite mining soils in Chimakurthy, India. The mineral exploration of mining soils were identified by X-Ray Diffractometer (XRD) pattern analysis. However, the morphological features and quantitative HMs were detected by Scanning Electron Microscopy/Energy Dispersed Spectroscopy (SEM/...

Mucoadhesive polymeric (carbopol 934) suspension of ciprofloxacin was prepared by ultrasonication and optimized with the aim of developing an oral controlled release gastro-retentive dosage form. The qualitative analysis of the formulation was performed by fourier transform infrared spectroscopy (FTIR), Raman spectroscopy, X-ray powder diffraction (XRD), and scanning electron microscopy (SEM) a...