SiO2/ZnS core/shell nanostructures have been synthesized at room temperature by a simple wet chemical method. The prepared materials are characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), infrared spectroscopy (IR), UV–vis spectroscopic and transmission electron microscopy (TEM) studies. X-ray diffraction pattern exhibits peaks correspond to the cubic phase of ZnS. Th...

nanoparticles of the zno and tio2 were synthesized and the physicochemical properties of the compounds were characterized by ir, x-ray diffraction (xrd), scanning electron microscopy (sem) and transmission electron microscopy (tem). the xrd patterns of the zno and tio2 nanoparticles could be indexed to hexagonal and rutile phase, respectively. aggregated nanoparticles of zno and tio2 with spher...

The progress in (scanning) transmission electron microscopy has led to an unprecedented knowledge of the microscopic structure of functional materials at the atomic level. Additionally, although not widely used yet, electron holography is capable to map the electric and magnetic potential distributions at the sub-nanometer scale. Nevertheless, in-situ studies inside a (scanning) transmission el...

In this study, Ni/NiO nanocomposites were prepared using simple, environment-friendly and low-cost solid-state thermal decomposition method from nickel (II) Schiff base complex at 400 and 500°C for 3 hours. The Ni/NiO nanocomposites were characterized with Fourier transformed infra-red spectroscopy (FT-IR), X-ray powder diffraction (XRD), transmission electron microscopy (TEM) and X-Ray fluores...

cr2o3 nanoparticles were prepared using cr(no3)3.9h2o as starting material, triethanolamine (tea) as template and water as green solvent under microwave irradiation. the products were characterized by x-ray diffraction (xrd), transmission electron microscopy (tem), fourier transform infrared (ft-ir), photoluminescence (pl) and raman spectroscopy. the size distribution of individual particles we...

nano-sized titanium dioxide tio2 powder was prepared by new wet chemical route from its precursor titanium (iv) chloride (ticl4) as precursor with isopropoxy alcohol in presence of nitric acid under ambient condition. their morphologies, phase compositions and components of the tio2 nanoparticles were characterized by transmission electron microscopy (tem), field emission scanning electron micr...

Titania, single-doped and lanthanum-silver co-doped titania nanocomposite were coated on cellulosic and polyacrylonitrile fibers via sol–gel method. The prepared samples were evaluated using x-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive x-ray spectroscopy (EDX), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), photolumines...

Seventy consecutive lung fine needle aspirates (FNA) from 69 patients were examined by cytology/cell block histology, by transmission electron microscopy (TEM), and, where available, at histological follow up to determine the value of TEM in interpreting lung FNAs. Of 70 FNAs, 50 were suitable for TEM. Transmission electron microscopy was helpful in classifying seven of 10 poorly differentiated...

sphere-like shaped cobalt oxide nanoparticles (co3o4) were synthesized by a simple wet chemical method using cobalt chloride as precursor and cetyl trimethylammonium bromide (ctab) as surfactant. their structural and surface morphologial properties were characterized by high resolution transmission electron microscopy (hrtem), field emission scanning electron microscopy (fesem) and x-ray diffra...

electrosynthesis process has been used for preparation of zinc sulfide nanoparticles. zinc sulfide nanoparticles in different size and shapes were electrodeposited by electrolysis of zinc plate as anode in sodium sulfide solution. effects of several reaction variables, such as electrolysis voltage, sulfide ion concentration as reactant, stirring rate of electrolyte solution and temperature on p...