Structural features of La(1-x)SrxMn0.5Co0.5O3 (x = 0.0, 0.1, 0.2, 0.3, 0.4, and 0.5) nano-particles were investigated using X-ray powder diffraction and FT-IR spectroscopy. The characterization of compounds by X-ray powder diffraction and using Fullprof program show a cubic structure (Pm3m space group) for x = 0.0 and a rhombohedra structure (R-3c space group) for the Sr substituted La(1-x)SrxM...