نتایج جستجو برای: x ray powder diffraction xrd
تعداد نتایج: 737007 فیلتر نتایج به سال:
in this study, amino functional groups were chemically bonded to the surface of newly synthesized kit-6 mesoporous magnetite nanoparticles (mmnps) by post-toluene reflux synthesis method. this method treats calcined mesoporous nanoparticles with the functional organosilanes. physical and chemical structures of the synthesized mesoporous magnetite nanoparticle...
In the present study, new multi-components spinel ferrite Zinc doped metallic ferrites are investigated. The synthesized compounds consisting of Zinc copper ferrite nanostructures were developed using the Co-precipitation technique. Powder X-ray diffraction pattern (XRD) confirms the formation of the spinel phase for all the samples. The lattice constant was studied through powder X-ray diffrac...
In this article the main possibilities of single crystal and powder diffraction analysis using conventional laboratory x-ray sources are introduced. Several examples of applications with different solid samples and in different fields of applications are shown illustrating the multidisciplinary capabilities of both techniques. Handbook of instrumental techniques from CCiTUB X-ray single crystal...
The use of plant extract is generating interest of researchers toward cost effective and eco-friendly green synthesis of nanoparticles. In the present work, Cupric oxide nanoparticles were synthesized using coffee powder extracts by the sol-gel method at different calcination temperatures. The synthesized nanoparticles were characterized by X-ray diffraction, scanning electron microscopy , ultr...
we evaluated the effect of fe/alumina catalyst contained different cadmium contents and two synthesis temperatures on producing carbon nanotubes by chemical vapor deposition of methane as a feedstock. x-ray powder diffraction (xrd), n2 adsorption-desorption, scanning electron microscopy (sem), transmission electron microscopy (tem), raman spectroscopy and thermogravimetry analysis (tga) were u...
in this work, we report on the synthesis of superparamagnetic iron oxide nanoparticles at room temperature using microemulsion template phase consisting of cyclohexane, water, ctab as cationic surfactant and butanol as a cosurfactant. surface modification have been carried out by using poly(ethyleneglycol) (peg). the structure,morphology, and magnetic properties of the products were characteriz...
Nickel oxide (NiO) nano-particles were produced via a rapid microwave-assisted method. Ni(OH)2 precursor was obtained by slow drop-wise addition of 0.1M sodium hydroxide to 0.1M nickel nitrate. The mixture was vigorously stirred until the pH reached 7.2. The mixture was then irradiated with microwave to deposit Ni(OH)2 at an intensified precipitation rate. Drying of the precipitate at 320°C res...
nanotechnology is a general term which is related with field of all advanced science term that generally predicates with all modern technologies which consider nanoscales. improvement in the quality of products by adding some nanoparticles and study of their behavior in the presence of these nanoparticles have been obtained in many researches. on the other hand numerous demands for sowing ...
The fixation of heavy metals (Ba, Cu, Pb) in an alkali-activated matrix was investigated. The matrix consisted of fly ash and blast furnace slag (BFS). The mixture of NaOH and Na-silicate was used as alkaline activator. Three analytical techniques were used to describe the fixation of heavy metals-X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM) equipped with energy di...
Microstructural, topology, inner morphology, and gas-sensitivity of mixed xWO(3)(1-x)Y(2)O(3) nanoparticles (x = 1, 0.95, 0.9, 0.85, 0.8) thick-film semiconductor gas sensors were studied. The surface topography and inner morphological properties of the mixed powder and sensing film were characterized with X-ray diffraction (XRD), atomic force microscopy (AFM), transmission electron microscopy ...
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