The Boehm titration, originally developed to characterize carbon blacks and activated carbons, has earned growing attention as a method for characterization of acid and base properties of biochar (Boehm, 1994; Goertzen et al., 2010). The method is based on the principle that strong acids and bases will react with all bases and acids, respectively, whereas the conjugate bases of weak acids will ...

As two important physico-chemical parameters, the acidic and alkaline residues of protein are of evident significance for the evaluation of protein properties and the design of relevant separation and analysis. However, there is still no electrophoretic method used for the direct detection of free acidic and alkaline residues of protein. Herein, we developed the concepts of moving reaction boun...

An automated procedure for photometric titration of red wine and associated instrumentation is described. The procedure was based on the flow-batch approach implemented employing multicommutation. The photometric detection was carried out using a homemade LED-based photometer. The mixing device, LED, and photodetector were attached to the titration chamber in order to form a compact and small-s...

Introduction In 1974 Fleet and Ho 1] successfully demonstrated an automated continuous flow titration system using a reagent gradient. This system had a throughput of only ten samples per hour, but it was significant since it demonstrated the principles for titration of discrete samples in continuously flowing streams. Nagy et al. [2,3 ]have also demonstrated a similar approach. In 1977, Ruzick...

STUDY AIM To evaluate the feasibility of combined oximetry (pulse oximetric saturation [Spo(2)]) and cutaneous capnography (transcutaneous carbon dioxide tension [Ptcco(2)]) for oxygen titration in patients requiring long-term oxygen therapy. METHODS Twenty patients with obstructive or restrictive lung disease underwent oxygen titration using a combined cutaneous oximetry-capnography sensor. ...

BACKGROUND Continuous oxygen treatment is essential for managing children with hypoxemia, but access to oxygen in low-resource countries remains problematic. Given the high burden of pneumonia in these countries and the fact that flow can be gradually reduced as therapy progresses, oxygen conservation through routine titration warrants exploration. AIM To determine the amount of oxygen saved ...

From the analysis of the potentiometric titration data of polyelectrolytes, we can obtain the electrostatic free energy of the macromolecules. Therefore, potentiometric titration is a useful experimental procedure to study the conformation and conformational change of macromolecules. A few examples of the application of potentiometric titration to the studies on polypeptides, protein and DNA ar...

PURPOSE We sought to better understand how dose and titration with duloxetine treatment may impact tolerability and treatment discontinuation in patients with major depressive disorder. PATIENTS AND METHODS We investigated Phase III duloxetine trials. Group 1 was a single placebo-controlled study with a 20 mg initial dose and a slow titration to 40 and 60 mg. Group 2 was a single study with a...