The corrosion behavior of Ti60 alloy covered with a solid NaCl deposit in wet oxygen flow at 600 °C has been studied further by SEM, EDX, XPS, XRD, TEM and EPMA analysis. The results show that solid NaCl and H2O react with Ti oxides, which destroyed the Ti oxide scale to yield the non-protective Na4Ti5O12 and other volatile species. The resulting corrosion product scale was multilayered and con...

A single-step approach for the synthesis of multi-walled nanotubes (MWNT) filled with nanowires of Ni/ternary Zr based hydrogen storage alloy has been illustrated. We also demonstrate the generation of COfree hydrogen by methane decomposition over alloy hydride catalyst. The present work also highlights the formation of single-walled nanotubes (SWNT) and MWNTs at varying process conditions. The...

In this study, PMAs/NiFe2O4 nanocomposite was prepared using in-situ polymerization technique. The structure and morphological properties of nano composited were determined via FT-IR, SEM, EDX analysis methods. Thermal properties of prepared nanocomposites were investigated by TGA, DTA and DSC. Pure NiFe2O4 nanoparticles were synthesized using hydrothermal synthesis using the same conditions wi...

ZnFe2O4 nanocomposites have been prepared by a simple co‐precipitation method. The prepared samples were characterized by Scanning Electron Microscopy (SEM), Powder X‐ray Diffraction (XRD), Energy Disperse X‐ray Analysis (EDX), Transmission electron microscopy (TEM) and UV‐visible absorption spectral techniques. Conductivity measurements show a transition from ferrimagnetism to...

In the present study, synthesis, characterization, and the antibacterial activity of silver nanoparticles from native isolate of Corynebacterium glutamicum has been reported. Silver nanoparticles were synthesized by challenging the dried biomass of C. glutamicum with aqueous diamine silver ([Ag (NH3)2]+) containing 1 mM AgNO3. Synthesized silver nanoparticles (AgNPs) were characterized by ultra...

An Egyptian, plant pathogenic Fusarium solani isolate was grown on cobalt concentrations of 0, 50, 200, 500, 800, and 1000 ppm. The isolate survived concentrations up to 800 ppm, however failed to grow at 1000 ppm. Morphology and elemental analysis of the isolate under the investigated Co concentrations were studied using Scanning electron microscopy (SEM) and energy dispersive X-ray microanaly...

Thermally evaporated silver nanoparticles on conducting substrates spontaneously evolve in size when immersed in pure water. The process was studied using scanning electron microscopy (SEM), energy-dispersive X-ray analysis (EDX), and optical absorption spectroscopy. The particles are proposed to reform through an electrochemical Ostwald ripening mechanism driven by the size dependence of the w...

Segmentation methods, combining spectral and spatial information, are essential for analysis of multi-spectral images. In this article, we propose such a method based on statistical pattern recognition algorithms and a combined classifier approach. A set of experiments is presented with multi-spectral images of detergent laundry powders acquired by imaging cross-sections with scanning electron ...

Single-crystalline SnO2 microcubes were grown using the hydrothermal method without any catalyst. X-ray diffraction (XRD) patterns and energy dispersive X-ray (EDX) analysis verified that the cubes are tin dioxide SnO2. Their morphology and structure was studied by scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), and Raman 5m...