Received 10 April 2015 Accepted 11 October 2015 Available online 30 September 2015 In this work, structural and magnetic properties of the LaMnO3+δ compound prepared by citrate precursor method and annealed in the presence of oxygen are investigated. The structural characterization of LaMnO3+δ by X-ray powder diffraction and X‟pert package and Fullprof program provides evidence for a rhombohedr...

1928091 IJBAS-IJENS @ International Journals of Engineering and Sciences IJENS Abstract— NiZn ferrite with composition Ni0.8Zn0.2Fe2O4 was prepared by the self combustion technique. The samples were sintered at 750 °C and 950 °C and characterized by XRD, SEM and Raman spectroscopy. From the analysis of X-ray diffraction patterns, the single phase and good nanocrystalline of Ni0.8Zn0.2Fe2O4 part...

A mercury plating technique was used to determine the phases forming on experimental Ag-Sn-Cu alloy powders (with and without Pd) exposed to electrolytically deposited mercury. Four series of alloy powders were made: a) 1.5% Pd with 10-14% Cu (CU series); b) 1.0% Pd with 10-14% Cu (1PD series); c) 1.5% Pd with different ratios of Ag3Sn (gamma) to Ag4Sn (beta) with 12% Cu (AGSN series); and d) 9...

Tamarind seed polysaccharide (TSP), a natural polysaccharide extracted from tamarind seeds is used in the pharmaceutical, textile and food industries as a mucoadhesive polymer. This work aimed to extract TSP from tamarind seeds from three sources with two methods and characterized its physical and chemical properties. Kernel powder of tamarind seeds was slurried into a clear solution, set aside...

nanostructured iron oxide powder that has been recovered from waste pickling liquor unit of steel industry was studied for oxidation catalytic applications. in this research, the powder was characterized by x-ray diffraction (xrd) and transition electron microscopy (tem) for determination of phase structure, morphology and particle size. furthermore, the specific surface area of the powder was ...

A combination of gel-casting and polymeric foam infiltration methods is used in this study to prepare porous bodies of hydroxyapatite (HA), to provide a better control over the microstructures of samples. These scaffolds were prepared by impregnating a body of porous polyurethane foam with slurry containing HA powder, and using a percentage of solids between 40% and 50% w/v, and three different...

This paper explores the capability of using the DFT-D ab initio random structure searching (AIRSS) method to generate crystal structures of organic molecular materials, focusing on a system (m-aminobenzoic acid; m-ABA) that is known from experimental studies to exhibit abundant polymorphism. Within the structural constraints selected for the AIRSS calculations (specifically, centrosymmetric str...

Poorly water-soluble drugs often suffer from limited or irreproducible clinical response due to their low solubility and dissolution rate. In this study, organic solvent-free solid dispersions (OSF-SDs) containing telmisartan (TEL) were prepared using polyvinylpyrrolidone K30 (PVP K30) and polyethylene glycol 6000 (PEG 6000) as hydrophilic polymers, sodium hydroxide (NaOH) as an alkalizer, and ...

The aim of this study is to fabricate high strength calcium phosphate/ yttrium artially stabilised zirconia (Y-PSZ) composites using a simple powder pressing technique. Various compositions of hydroxyapatite and zirconia powder, ranging from 10 to 90 wt% Y-PSZ, were prepared using a wet mixing process. Ten compacts (13.5mm×3mm) were made for each composition, pressed and fired in air at sinte...

Zuotai (gTso thal) is one of the famous drugs containing mercury in Tibetan medicine. However, little is known about the chemical substance basis of its pharmacodynamics and the intrinsic link of different samples sources so far. Given this, energy dispersive spectrometry of X-ray (EDX), scanning electron microscopy (SEM), atomic force microscopy (AFM), and powder X-ray diffraction (XRD) were u...