نتایج جستجو برای: energy dispersion x ray spectroscopy eds

تعداد نتایج: 1452104  

2016
Mohammad Aghazadeh Meshgi Manfred Kriechbaum Subhajit Biswas Justin D Holmes Christoph Marschner

The synthesis of size-monodispersed indium nanoparticles via an innovative simultaneous phase transfer and ripening method is reported. The formation of nanoparticles occurs in a one-step process instead of well-known two-step phase transfer approaches. The synthesis involves the reduction of InCl3 with LiBH4 at ambient temperature and although the reduction occurs at room temperature, fine ind...

Journal: :Nanoscale 2014
Qingsheng Liu Agustín Díaz Andrey Prosvirin Zhiping Luo James D Batteas

Two different nickel precursors (NiCl2 or Ni(CH3COCH2COCH3)2) in the presence of 1-dodecanethiol and a mixture of oleylamine and oleic acid were used for a one-pot colloidal synthesis to produce high purity Ni3S4 nanoparticles with controlled shapes in high yields and narrow size distributions. By simply changing the nickel precursors, the shape of Ni3S4 nanocrystals can be readily tuned from t...

2017
Krzysztof Rokosz Tadeusz Hryniewicz Steinar Raaen

Original scientific paper Plasma Electrolytic Oxidation (PEO) of NiTi alloy was studied in the electrolyte consisting generally of concentrated orthophosphoric acid with an addition of copper II nitrate. The PEO process was used to obtain a nanostructured coating on the Nitinol surface. The surface layer analyses methods, such as scanning electron microscopy (SEM) with the energy-dispersive X-r...

2014
Marcia Regina Salvadori Cláudio Augusto Oller Nascimento Benedito Corrêa

The synthesis of nickel oxide nanoparticles in film form using dead biomass of the filamentous fungus Aspergillus aculeatus as reducing agent represents an environmentally friendly nanotechnological innovation. The optimal conditions and the capacity of dead biomass to uptake and produce nanoparticles were evaluated by analyzing the biosorption of nickel by the fungus. The structural characteri...

In this study, immobilized CuAlO2 onto the ZSM-12&35 composite was prepared and used as a photocatalyst to remove N-containing oil pollutants (Carbazole) through advanced oxidation. In this method, acetone is used as a reaction solvent that can be partially converted to fuel oxygenates compounds (Octane enhancers) through an aldol condensation reaction. Photocatalyst characterization was perfor...

Bahar Khodadadi Mohammad Sabeti Omulbanin Norozi

For the first time the extract of the plant of Tilia platyphyllos was used to green synthesis of Ag nanoparticles (NPs) supported on Ziziphus jujuba kernel as an environmentally benign support. Ag NPs/ Ziziphus  jujuba  kernelas  an  effective  catalyst  was  prepared  through reduction  of Ag+ions using Tilia  platyphyllos extractas  the  reducing  and capping agent  and Ag  NPs immobilization...

Silver nanowires (AgNWs) are considered as one-dimensional nanostructures, which have received much attention due to their nanoscale size, high aspect ratio, high electrical and thermal conductivity, optical transparency and high mechanical stability. Preparation of AgNWs by polyol process is remarkably sensitive to the interactions between synthesis parameters. In this study, the effect of the...

In this research the synthesis of [Co(Salen)(PPh3)(H2O)]4[Fe(CN)6] and [Co(Salophen)(PPh3)(H2O)]4[Fe(CN)6] schiff base complexes was reported. Co3O4/CoFe2O4 magnetic nanoparticles were prepared by calcination of these complexes at 500, 550 and 600°C. Precursor complexes were identified by FT-IR and UV-Vis spectroscopy and their thermal behavior was studied via TG/DTA. Nanomagnetic samples were ...

The effect of rare earth (RE) elements, including Ce and La, on the sorption properties of Zr-Co getters was investigated in this work. The phase evolution, microstructural characteristics of getter powders were studied by means of X-ray diffraction method, scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS). The nanostructured Zr3Co intermetallic compound has been...

H. H. Hanish, M. M. Shukur S. J. Edrees

Pure and doped magnesium oxide nanoparticles were successfully synthesized employing a sol-gel process. The synthesized nanoparticles were characterized by thermal differential analysis, X-ray powder diffraction, transmission electron microscopy, scanning electron microscope, energy-dispersive X-ray spectroscopy, and vibrating sample magnetometer. X-ray diffraction patterns confirmed the crysta...

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