Zinc in pooled human serum, diluted 10-fold with demineralized water, was determined by flame atomic absorption spectrophotometry. Recoveries of zinc added to the serum were calculated by use of standards prepared in water, physiological saline, synthetic serum, or dilute HNO3 (10 ml/liter). The flow rates were essentially the same (9.1 to 9.3 ml/min) for water, diluted synthetic serum or act...

We introduce hybrid solar cells with an architecture consisting of an electrodeposited ZnO nanorod array (NRA) coated with a conformal thin layer (<50 nm) of organic polymer-fullerene blend and a quasi-conformal Ag top contact (Thin/NR). We have compared the performance of Thin/NR cells to conventional hybrid cells in which the same NRAs are completely filled with organic blend (Thick/NR). The ...

Zinc oxide nanofibers were prepared using the polymer Zinc acetate solution, by a modest programmable microcontroller aided electro spinning technique. The prepared and calcinated nanofibers were characterized using standard analytical methods. The hexagonal wurtzite structure for calcinated nanofibers of diameters ranging between 10-13 nm were inferred from structural analysis. The Field Emiss...

The ability to precisely control interfaces of atomic layer deposited (ALD) zinc oxysulfide (Zn(O,S)) buffer layers to other layers allows precise tuning of solar cell performance. The O K- and S K-edge X-ray absorption near edge structure (XANES) of ∼2-4 nm thin Zn(O,S) films reveals the chemical and structural influences of their interface with ZnO, a common electrode material and diffusion b...

This work reports an x-ray absorption near-edge structure spectroscopy (XANES) study at both Mn and Zn K edges in Zn(0.95)Mn(0.05)O thin films prepared with different sputtering gases (pure Ar, Ar/N(2) and Ar/O(2)). We have studied the local order around Mn in the films, with special emphasis on the role played by both oxygen and zinc vacancies and by the structural distortion associated with t...

The synthesis of ZnO nanoparticles has attracted considerable interest because of their unique properties and potential applications in a variety of solid state devices, catalytic media etc. By using water-in-oil (w/o) microemulsions, nanodroplets of water were used as chemical reactor to synthesize nanoparticles of zinc oxide. Addition of reducing agent ((NH4)2CO3) and zinc salt (Zn(NO3)2) fol...

We measured zinc in the plasma of 50 normal persons, and in erythrocytes of six, by an automated micromethod of atomic absorption spectrometry. Using a rotation viscometer, we measured the viscosity and flow behavior of plasma, undiluted and equi-volume diluted (with water), from 12 patients, and, for comparison, of two- to 20-fold dilutions of an 870 mL/L glycerol solution. Erythrocytes were w...

The initial purification of metallothionein from equine renal cortex yielded preparations that were electrophoretically heterogeneous and contained 2.9% cadmium, 0.6% zinc, and 4.1% sulfur (1). By diethylaminoethyl cellulose column chromatography, we have now obtained electrophoretically and ultracentrifugally homogeneous metallothionein containing 5.9 ‘% cadmium, 2.2% zinc, and 8.5% sulfur. Mo...

Through the microwave assisted fast synthesis method, Zinc Magnesium Oxide nanocomposite was prepared. Zinc Magnesium Oxide nanocomposite heated at 500oC was used for further structural, optical and antibacterial studies. The Debye Scherrer equation was used to calculate the average particle size of the nanocomposite. The optical characterization of the oxide nanocomposite was carried out by UV...

A new micromethod for the determination of copper and zinc is presented. Sample volumes can be as little as 10 (Cu) and 20 (Zn) microliter of plasma or serum, by using discrete (small sample volume) nebulization in place of conventional nebulization in place of conventional nebulization in atomic absorption spectrometry. The present method has slightly poorer precision than the conventional neb...