نتایج جستجو برای: crystallite size determination
تعداد نتایج: 795243 فیلتر نتایج به سال:
The synthesis of nano-sized particles of NU-1000 (length from 75 nm to 1200 nm) and PCN-222/MOF-545 (length from 350 nm to 900 nm) is reported. The catalytic hydrolysis of methyl paraoxon was investigated as a function of NU-1000 crystallite size and a significant enhancement in the rate was observed for the nano-sized crystals compared to microcrystals.
we develop a two phase sampling procedure to determine the sample size necessary to estimatethe population mean of a normally distributed random variable and show that the resulting estimator has preassigned variance and is unbiased under a regular condition. we present a necessary and sufficient condition under which the final sample mean is an unbiased estimator for the population mean.
YVO4:Eu nanocrystals synthesized by direct precipitation reaction. The morphologic transformation of the nanocrystals as the results of thermal treatments were analyzed using optical spectroscopy. A red shift of the fluorescence lines with the increase of the crystallite size was observed. The kinetics of the D0 level of Eu3+ is also analyzed.
Fe2O3-Al2O3 compounds with different Fe/Al compositions were synthesized by coprecipitation (CP) method and calcined at 300°-1000°C. The formation of crystalline phases (e.g., maghemite, hematite), transformation temperature, specific surface area, lattice parameter, crystallite size, magnetic properties of iron oxide were all affected by the component ratio and thermal treatment.
Although Cu and Fe are immiscible under equilibrium conditions, they can form supersaturated solid solutions by mechanical alloying. In this paper, nano-structured of the metastable Cu-Fe phase containing 10, 15, 20 and 25% wt Fe were synthesized by intensive ball milling for 15h, in order to achieve a solid solution of Fe in Cu. The phase composition, dissolution of the Fe atoms into the Cu ma...
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