The conventional ceramic route was utilized to prepare a hard magnetic powder (M-type strontium ferrite, SrFe12O19). The stoichiometric mixture of iron oxide and strontium carbonate were calcined at 1000C and then fired at various temperatures. The influence of various reaction parameters such as mixing ratio, calcination temperature, firing temperature and firing time on the magnetic behaviors...

Synthetic fluorspar can be produced from waste calcium fluoride slurry settled on dumpsites located near Cracow centre. Synthetic fluorspar exchanges natural raw material used in the metallurgical industry. To obtain grained synthetic fluorspar, calcium fluoride slurry should be calcinated in rotary kilns at temperatures of 900-1100K. Grain size and compression strength strongly depends on calc...

lini0.5co0.5vo4 has been successfully synthesized by tartate precursor combustion method using li2co3, co(no3)2.6h2o, ni(no3)2.6h2o and nh4vo3 as a starting materials in deionized water with the subsequent calcination at 450-600 oc for 12 h. the combustion and decomposition of tartate precursor were studied by tga and compared with tartaric acid. it found weight loss at 50-450 oc. the product s...

as a new precursor, [tris(2-hydroxyacetophenato) triaqua(iii)], [y(hap)3(h2o)3]; complex was used in thermal decomposition process for the synthesis of rod-like high-temperature ceramic ybco with length of about 320-350 nm and diameters 60–90 nm. the as-synthesized products were characterized by xrd, ft-ir, tem, sem and edx analyses. the results showed that by using fine raw materials, the calc...

Nanostructured alumina thin films were coated on stainless steel by Sol-Gel dip coating method. In order to prevent crack formation, Al2O3 films were kept in a solvent bath immediately after coating to reduce the rate of drying. Effects of calcination temperature and withdrawal speed on structural properties were analyzed using XRD and SEM. Topography and thickness of coat...

tio2 nanoparticles were synthesized by modified sol—gel method using pure room temperature ionic liquid(rtil) 2-hydroxyethylammonium formate as a reaction medium. the structure and morphology of tio2nanoparticles were characterized with x-ray powder diffraction (xrd), bet surface analysis and scanningelectron microscopy (sem). tio2 nanoparticles were synthesized in open and closed vessels. the ...