Abstract Herein, we present a detailed study of the structural, optical, and electrochemical responses Gd 2 O 3 doped with nickel zinc ferrite nanoparticles. Doping Ni 0.5 Zn Fe 4 nanoparticles to powder was done through thermal decomposition at 1000 °C. The average grain size mixture determined be approximately 95 nm, phases cubic , GdO, orthorhombic prisms GdFeO were identified. focused ion b...